A new method, microwave-induced combustion synthesis, was developed so as to
produce highly sinterable Y2O3-doped CeO2 nanopowders. The process took only
0.25h to yield Y2O3-doped CeO2 powders. An investigation was also made of the
conductivity of Y2O3-doped CeO2 ceramics. It was found that the Y2O3
concentration had a large effect upon the morphology, activation energy, ionic
conductivity and mechanical properties of Y2O3-doped CeO2 ceramics. The results
revealed that the bulk densities of Y2O3-doped CeO2 ceramics sintered at 1420C
for 5h were all higher than 92% of the theoretical densities, and that the maximum
ionic conductivity at 800C was 0.023S/cm, the minimum activation energy was
0.954eV, at 300 to 800C and that the maximum fracture toughness of
1.825MPam1/2 was found for 9mol%Y2O3-doped CeO2 specimens. The grain size
of CeO2 decreased with increasing Y2O3 concentration. The fracture toughness was
found to increase with increased Y2O3 concentration; because of the decrease in
CeO2 grain size.
Ionic Conductivity and Mechanical Properties of Y2O3-Doped CeO2 Ceramics
Synthesis by Microwave-Induced Combustion. Y.Fu: Ceramics International, 2009,
35[2], 653-9