Raman studies of Fe3O4 films of various thicknesses, grown onto single-crystal Si
and MgO substrates were used to investigate the presence of antiphase boundaries.
The X-ray diffraction and X-ray photo-electron spectroscopy measurements
indicated that the films were single-phase Fe3O4 on both substrates. The changes in
frequency and line-width of various Raman modes [A1g and T2g(3)] were
monitored, and the electron-phonon coupling parameter was computed. The latter
was correlated with the combined effect of strain and antiphase boundaries present
in the films and it was concluded that films grown on Si substrates were free from
antiphase boundaries. Probing Antiphase Boundaries in Fe3O4 Thin Films Using Micro-Raman
Spectroscopy. S.Tiwari, D.M.Phase, R.J.Choudhary: Applied Physics Letters,
2008, 93[23], 234108