It was found that the inward diffusion of network-modifying divalent cations could
occur in iron-containing silicate glasses when they were treated in a reducing
atmosphere near to the glass transition temperature. As a result of the inward
diffusion, a silica-rich nanolayer formed on the glass surface and increased the
hardness and chemical durability. The thickness of the layer could be controlled by
varying the heat-treatment conditions. The mechanism of inward diffusion was
clarified and the diffusion coefficient for the network-modifying divalent cations
was calculated. It was demonstrated that the diffusion of these ions was the ratelimiting
factor in the reduction process.
Inward Cationic Diffusion in Glass. M.M.Smedskjaer, Y.Z.Yue: Journal of Non-
Crystalline Solids, 2009, 355[14-15], 908-12