The tracer diffusion of O was measured mainly in the c-axis direction of monocrystalline samples, at temperatures of between 300 and 650C, by using secondary ion mass spectrometry. Other measurements were made of diffusion on the ab-plane of twinned crystals and in the b-axis direction of non-twinned crystals. It was found that the diffusivity in the c-axis direction was about 106 times lower than the diffusivity in polycrystals at 400C. The diffusivity in the b-axis direction was at least 100 times faster than that in the a-axis direction at 300C. Within an experimental uncertainty of a factor of 2, the O diffusivity in polycrystals was independent of the O partial pressure at 400C.
Anisotropy of Oxygen Tracer Diffusion in Single-Crystal YBa2Cu3O7-δ. S.J.Rothman, J.L.Routbort, U.Welp, J.E.Baker: Physical Review B, 1991, 44[5], 2326-33
Table 62
Diffusivity of 18O in Cu3Ba2YO7
Temperature (C) | PO2 (MPa) | Component | D (cm2/s) |
300 | 0.1 | fast | 3.96 x 10-13 |
300 | 0.1 | fast* | 1.11 x 10-12 |
300 | 0.1 | slow | 1.62 x 10-14 |
300 | 0.1 | slow* | 1.72 x 10-13 |
391 | 0.1 | fast* | 2.61 x 10-11 |
391 | 0.1 | slow* | 1.52 x 10-12 |
400 | 0.1 | fast | 7.35 x 10-12 |
400 | 0.1 | slow | 2.81 x 10-13 |
600 | 0.1 | fast | 2.80 x 10-10 |
600 | 0.1 | fast* | 1.29 x 10-10 |
600 | 0.003 | fast | 2.23 x 10-10 |
600 | 0.02 | fast | 1.62 x 10-10 |
652 | 0.1 | fast | 8.00 x 10-10 |
711 | 0.1 | fast | 1.38 x 10-9 |
780 | 0.1 | fast | 2.49 x 10-9 |
850 | 0.1 | fast | 6.33 x 10-9 |
*material with up to 4at% of excess Cu