Single crystals and polycrystalline electrolytic material was studied. The diffusion coefficient was deduced, at temperatures of 233 to 303K, from the frequency-dependence of the phase difference between anodic permeation
current and cathodic charging current. The results could not be described by an Arrhenius relationship (figure 3). Trapping effects were significant, at low temperatures, in both polycrystalline and monocrystalline crystals.
Y.Hayashi, M.Nagano, N.Ohtani: Nippon Kinzoku Gakkaishi, 1980, 44[1], 48-52
Table 30
Apparent Diffusivities of H in Fe
of Various Degrees of Purity at 25C
Material | D (cm2/s) |
high-purity (4N85) Fe | 4.08 x 10-6 |
electrolytic (2N87) Fe, 400ppmO | 2.8 x 10-6 |
electrolytic (2N87) Fe, 150ppmO | 2.85 x 10-6 |
Armco (2N5) Fe | 3.9 x 10-7 |
high-purity Fe, 0.04wt%Ni | 4.56 x 10-6 |
electrolytic Fe, 0.09wt%Ni | 1.34 x 10-6 |
high-purity Fe, 0.15wt%Ni | 1.22 x 10-6 |
electrolytic Fe, 0.5wt%Ni | 1.14 x 10-6 |
high-purity Fe, 0.9wt%Ni | 9.8 x 10-7 |
electrolytic Fe, 1.7wt%Ni | 8.07 x 10-7 |
electrolytic Fe, 2.5wt%Ni | 8.2 x 10-7 |