The capillary reservoir technique was used to study the diffusion of 22Na in molten mixtures (table 180). It was suggested that AlF63-, AlF4-, NaF and Na2F+ complexes were present in the melt. The activation energy for 22Na diffusion in samples with 13.5mol%AlF3, at temperatures ranging from 938 to 1070C, was 9.5kcal/mol. The activation energy for diffusion in samples with 37.5mol%AlF3, at 928 to 999.7C, was 7.0kcal/mol. Na-22 and F-18 Diffusion in Na and Al Fluoride Baths. D.Harari, F.Lantelme, M.Chemla: Journal de Chimie Physique et de Physicochimie Biologique, 1969, 66[7-8], 1286-91
Table 180
Self-Diffusion of 22Na in NaF-AlF3 Melts
AlF3 (mol%) | Temperature (C) | D (cm2/s) |
0 | 1049 | 9.80 x 10-5 |
0 | 1052 | 1.00 x 10-4 |
13.5 | 938 | 6.82 x 10-5 |
13.5 | 944.5 | 7.65 x 10-5 |
13.5 | 1012 | 8.17 x 10-5 |
13.5 | 1051 | 1.06 x 10-4 |
13.5 | 1070 | 1.03 x 10-4 |
25.0 | 1048 | 9.30 x 10-5 |
25.0 | 1049.5 | 9.44 x 10-5 |
25.0 | 1054 | 9.36 x 10-5 |
37.5 | 928 | 8.31 x 10-5 |
37.5 | 941 | 8.05 x 10-5 |
37.5 | 968.5 | 9.39 x 10-5 |
37.5 | 999.7 | 1.02 x 10-4 |