A pulsed-field gradient nuclear magnetic resonance spin echo technique was used to measure the diffusivities in TaHx. It was found that the activation energy increased with increasing H concentration, whereas the pre-exponential factor was not markedly concentration-dependent:
TaH0.12: D (cm2/s) = 3.1 x 10-4 exp[-0.143(eV)/kT]
TaH0.17: D (cm2/s) = 4.6 x 10-4 exp[-0.164(eV)/kT]
TaH0.34: D (cm2/s) = 3.5 x 10-4 exp[-0.162(eV)/kT]
TaH0.38: D (cm2/s) = 4.1 x 10-4 exp[-0.170(eV)/kT]
TaH0.52: D (cm2/s) = 4.3 x 10-4 exp[-0.182(eV)/kT]
TaH0.74: D (cm2/s) = 2.6 x 10-4 exp[-0.170(eV)/kT]
TaH0.77: D (cm2/s) = 3.3 x 10-4 exp[-0.183(eV)/kT]
The results were not consistent with the random occupation of tetrahedral sites.
P.E.Mauger, W.D.Williams, R.M.Cotts: Journal of the Physics and Chemistry of Solids, 1981, 42[9], 821-6