The tracer diffusivity of 18O was determined, at temperatures of between 300 and 850C, by using secondary ion mass spectrometry. It was found that the diffusion of O was markedly anisotropic (table 61). The faster-diffusing component, for migration in the ab-plane, was associated with an activation energy of 0.97eV. There was no break in the Arrhenius plot at the orthorhombic to tetragonal transformation temperature. The diffusion coefficient at 600C was not a sensitive function of O partial pressures ranging from 3kPa to 0.1MPa.
S.J.Rothman, J.L.Routbort, J.E.Baker: Physical Review B, 1989, 40[13], 8852-60
Table 61
Diffusivity of 18O in Cu3Ba2YO7
Temperature (C) | PO2 (MPa) | Component | D (cm2/s) |
300 | 0.1 | fast | 3.96 x 10-13 |
300 | 0.1 | fast* | 1.11 x 10-12 |
300 | 0.1 | slow | 1.62 x 10-14 |
300 | 0.1 | slow* | 1.72 x 10-13 |
391 | 0.1 | fast* | 2.61 x 10-11 |
391 | 0.1 | slow* | 1.52 x 10-12 |
400 | 0.1 | fast | 7.35 x 10-12 |
400 | 0.1 | slow | 2.81 x 10-13 |
600 | 0.1 | fast | 2.80 x 10-10 |
600 | 0.1 | fast* | 1.29 x 10-10 |
600 | 0.003 | fast | 2.23 x 10-10 |
600 | 0.02 | fast | 1.62 x 10-10 |
652 | 0.1 | fast | 8.00 x 10-10 |
711 | 0.1 | fast | 1.38 x 10-9 |
780 | 0.1 | fast | 2.49 x 10-9 |
850 | 0.1 | fast | 6.33 x 10-9 |
*material with up to 4at% of excess Cu