The diffusion of O in undoped and Ag-doped single crystals was investigated by performing isothermal resistivity measurements at temperatures ranging from 550 to 750C. It was found that the diffusion coefficients for Ag-doped crystals were an order of magnitude lower than those for undoped ones (table 62). Furthermore, the activation energy for O diffusion was found to be considerably higher for Ag-doped crystals. Further analysis of the data indicated that doping with Ag stabilized the phase at higher O contents.
D.K.Aswal, S.K.Gupta, P.K.Mishra, V.C.Sahni: Superconductor Science and Technology, 1998, 11[7], 631-6
Table 62
Diffusivity of O in Cu3Ba2YO7
Sample | Experiment | Temperature (C) | D (cm2/s) |
undoped | in-diffusion | 550 | 2.77 x 10-6 |
undoped | in-diffusion | 600 | 5.20 x 10-6 |
undoped | in-diffusion | 650 | 9.24 x 10-6 |
undoped | out-diffusion | 550 | 1.66 x 10-6 |
undoped | out-diffusion | 600 | 2.77 x 10-6 |
undoped | out-diffusion | 650 | 4.16 x 10-6 |
Ag-doped | in-diffusion | 650 | 2.89 x 10-7 |
Ag-doped | in-diffusion | 700 | 8.03 x 10-7 |
Ag-doped | in-diffusion | 750 | 3.07 x 10-6 |
Ag-doped | out-diffusion | 650 | 1.01 x 10-7 |
Ag-doped | out-diffusion | 700 | 5.04 x 10-7 |
Ag-doped | out-diffusion | 750 | 1.96 x 10-6 |