A pulsed field gradient nuclear magnetic resonance spin-echo technique was used to measure diffusivities. The activation energy increased with increasing H concentration, whereas the pre-exponential factor was not greatly concentration-dependent (table 96). The results were not consistent with the random occupation of tetrahedral sites, and it was suggested that repulsive interactions existed between H atoms on nearest-neighbor sites.
P.E.Mauger, W.D.Williams, R.M.Cotts: Journal of the Physics and Chemistry of Solids, 1981, 42[9], 821-6
Table 96
Parameters for H Diffusion in NbHx
x | Do (cm2/s) | E (eV) |
0.10 | 3.2 x 10-4 | 0.115 |
0.33 | 4.9 x 10-4 | 0.142 |
0.55 | 1.0 x 10-3 | 0.168 |
0.70 | 7.2 x 10-4 | 0.174 |
0.89 | 5.6 x 10-4 | 0.164 |