The diffusion of Al-replacing elements was investigated (tables 12 and 13), over a wide temperature range, in single crystals with the composition: Ni75.9Al24.1. The concentration profiles were measured by means of secondary ion mass spectrometry. A model was suggested for minority-component diffusion, via anti-structure defects, in the L12 structure. It involved nearest-neighbor jumps of solute atoms on the Ni sub-lattice, as anti-structure atoms, and the formation of so-called anti-structure bridges which corresponded to jumps between different sub-lattices. The model was shown to agree with experimental data on Al-replacing solute diffusion, and it explained the observed ratio of the self- to solute-diffusivities. This ratio could be higher or lower than unity; depending upon the solute and upon the temperature.
Solute Diffusion of Al-Substituting Elements in Ni3Al and the Diffusion Mechanism of the Minority Component S.V.Divinski, S.Frank, U.Södervall, C.Herzig: Acta Materialia, 1998, 46[12], 4369-80
Table 12
Bulk Diffusion of Al-Replacing Solutes in Ni3Al Single Crystals
Diffusant | Temperature (K) | D (m2/s) |
Ga | 1005 | 9.93 x 10-21 |
Ga | 1053 | 5.95 x 10-20 |
Ga | 1080 | 3.51 x 10-19 |
Ga | 1176 | 5.31 x 10-18 |
Ga | 1278 | 9.52 x 10-17 |
Ga | 1320 | 3.89 x 10-16 |
Ga | 1370 | 1.04 x 10-15 |
Ga | 1422 | 3.90 x 10-15 |
Ge | 1047 | 4.30 x 10-20 |
Ge | 1090 | 2.11 x 10-19 |
Ge | 1154 | 2.53 x 10-18 |
Ge | 1226 | 2.05 x 10-17 |
Ge | 1306 | 2.45 x 10-16 |
Ge | 1355 | 5.30 x 10-16 |
Ti | 1090 | 5.05 x 10-21 |
Ti | 1158 | 5.48 x 10-20 |
Ti | 1222 | 4.45 x 10-19 |
Ti | 1256 | 1.65 x 10-18 |
Ti | 1306 | 1.12 x 10-17 |
Ti | 1385 | 7.55 x 10-17 |
Ti | 1453 | 5.59 x 10-16 |
Nb | 1157 | 8.81 x 10-21 |
Nb | 1216 | 1.10 x 10-19 |
Nb | 1254 | 3.10 x 10-19 |
Nb | 1300 | 2.18 x 10-18 |
Nb | 1327 | 5.31 x 10-18 |
Nb | 1372 | 1.73 x 10-17 |
Nb | 1408 | 5.48 x 10-17 |
Nb | 1444 | 1.84 x 10-16 |
Table 13
Arrhenius Parameters for Bulk Diffusion in Ni3Al
Diffusant | Do (m2/s) | Q (kJ/mol) |
Ga | 0.0787 | 363.1 |
Ge | 0.107 | 368.6 |
Ti | 0.859 | 424.6 |
Nb | 25.8 | 475.6 |