The pressure and temperature dependences of 63Ni heterodiffusion was investigated at temperatures ranging from 888 to 1282K (table 10). This range included the critical temperature of the A2-B2 order-disorder transition. A radio-tracer method was used, combined with a serial sectioning technique. The high-pressure measurements showed that the diffusion process was controlled by mono-vacancies in both the ordered and disordered structures. The Arrhenius plot exhibited a downward curvature, as a result of B2-type ordering, and the lattice diffusion coefficients could be fitted by a continuous curve as a function of temperature and long-range order parameter. Because of the preference of Ni for α-sites, the Ni diffusivity was slower and the activation energy for diffusion was higher than the corresponding values for Fe self-diffusion.
Pressure and Temperature Dependence of Nickel Diffusion in Fe3Al: Effect of Ordering Z.Tôkei, J.Bernardini, G.Erdélyi, I.Gôdény, D.L.Beke: Acta Materialia, 1998, 46[13], 4821-5
Table 10
Diffusion of 63Ni in Fe3Al
Temperature (K) | Structure | P (kbar) | D (m2/s) |
888 | B2 | 1.0 | 9.84 x 10-19 |
933 | B2 | 1.0 | 6.73 x 10-18 |
973.5 | B2 | 0.1 | 8.4 x 10-17 |
973.5 | B2 | 1.9 | 7.3 x 10-17 |
973.5 | B2 | 3.3 | 5.8 x 10-17 |
973.5 | B2 | 6.1 | 4.4 x 10-17 |
973.5 | B2 | 8.6 | 3.3 x 10-17 |
1028 | B2 | 1.0 | 2.60 x 10-16 |
1073 | A2 | 0.1 | 1.2 x 10-15 |
1073 | A2 | 0.6 | 1.7 x 10-15 |
1073 | A2 | 1.0 | 8.80 x 10-16 |
1073 | A2 | 1.0 | 1.08 x 10-15 |
1073 | A2 | 1.9 | 1.8 x 10-15 |
1073 | A2 | 4.0 | 8.9 x 10-16 |
1073 | A2 | 6.3 | 9.2 x 10-16 |
1073 | A2 | 8.5 | 8.0 x 10-16 |
1177 | A2 | 1.0 | 1.17 x 10-14 |
1282 | A2 | 1.0 | 6.84 x 10-14 |