Equal channel angular extrusion (ECAE) was employed in an attempt to develop nanostructural metal matrix composites with homogenized distribution of reinforcing particles. Zn- Al metal matrix composites reinforced with 5 μm SiC particulates were produced by casting method. A non-uniform distribution of the reinforcing particles was evident in the metal matrix. With repetitive shear deformation imposed via the ECAE process, substantial structural improvement was achieved and the reinforcing particulates were de-clustered into a finely dispersed distribution throughout the metal matrix. The homogeneity of the particle distribution was studied by the Quadrat method and the skew factors were determined. It was found that the skew factors were substantially reduced after 8 extrusion passes, showing the homogeneity of the particle distribution was greatly improved in the composites.