In Situ TiB Reinforced Titanium Metal Matrix Composites Prepared by Spark Plasma Sintering


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In situ synthesized TiB reinforced titanium matrix composites of Ti-B and Ti-TiB2 systems have been prepared by spark plasma sintering at 800-1200 °C under 20 MPa for 5 min. The effects of sintering temperature and reinforcement volume fraction on flexural strength, Young’s modulus and fracture toughness of the composites were investigated. The in situ synthesized TiB reinforcements are randomly and uniformly distributed in titanium matrix. The TiB whiskers are aligned along [010] direction, and the crystallographic planes of the TiB needles are always of the type (100), (101) and (10 1) . The parallel TiB were observed in β-Ti grains in both of the investigated composites. The in situ TiB needle is likely to grow along [010] direction which is parallel to [111] direction of cubic lattice of β-Ti phase.



Edited by:

Masaaki Naka and Toshimi Yamane




Y. Zhou et al., "In Situ TiB Reinforced Titanium Metal Matrix Composites Prepared by Spark Plasma Sintering ", Materials Science Forum, Vol. 502, pp. 189-194, 2005

Online since:

December 2005




[1] S.C. Tjong, K.C. Lau: Mater Sci Eng. A282 (2000), p.183.

[2] S. Ranganath, R.S. Mishra: Acta Metall Mater. 44 (1996), p.927.

[3] S. Debuy, W.O. Soboyejo, T.S. Srivatsan: Appl Comp Mater. 4 (1997), p.361.

[4] Z.J. Shen, M. Johnsson, M. Nygren: J Eur Ceram Soc. 23 (2003), p.1061.

[5] L.L. Ye, Z.G. Liu, K. Raviprasad, M.X. Quan, M. Umemoto, Z.Q. Hu: Mater Sci Eng. A241 (1998), p.290.

[6] S. Perera, M. Tokita, S. Moricca: J Eur Ceram Soc. 18 (1998), p.401.

[7] X.N. Zhang, W.J. Lu, D. Zhang, R.J. Wu: Scripta Mater. 41 (1999), p.39.

[8] W.J. Lu, D. Zhang, X.N. Zhang, R.J. Wu, T. Sakata, H. Mori: J Alloy Compd. 327 (2001), p.240.

[9] B.J. Kooi, Y.T. Pei, J. Th.M. De Hosson: Acta Mater. 51(2003), p.831.

[10] P. Mogilevsky, A. Werner, H.J. Dudek. Reactive formation of TiB at the TiB2-Ti interface, Defect and Diffusion Forum, Switzerland, Vols. 143-147, 1997, p.585.


[11] P. Mogilevsky, A. Werner, H.J. Dudek. Mater Sci Eng. A242 (1998), p.235.

[12] M. E. Hyman, C. McCullough, J. J. Valencia. C.G. Levi. R. Mehrabian. Metall. Trans. A20 (1989), p.1847. Fig. 11 Typical fractographs of 10vol. % TiB reinforced composites sintered at (a) 800 °C; (b) 1000 °C and (c) 1200 °C.

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