Improvement in Microstructure Homogeneity of Sintered Compacts through Powder Treatments and Alloy Designs


Article Preview

Homogeneous microstructures of the PM compacts are difficult to attain when mixed elemental powders are used. This study examined the microstructures of pressed-and-sintered and MIM products that contain Ni and Mo. Ni-rich areas, which were lean in carbon and were soft, were found easily in regular specimens. Gaps or cracks near the Ni-rich or Mo-rich areas were also frequently observed. This problem got worse when Ni and Mo particles were large and were irregular in shape. By using ball milling treatment and ferroalloy powders, the microstructure homogeneity and mechanical properties were improved. The addition of 0.5wt%Cr further improved the distribution of Ni because Cr reduced the repulsion effect between nickel and carbon. With the elimination of Ni-rich areas, more bainites and martensites were formed and mechanical properties were significantly improved.



Materials Science Forum (Volumes 534-536)

Edited by:

Duk Yong Yoon, Suk-Joong L. Kang, Kwang Yong Eun and Yong-Seog Kim




K.S. Hwang et al., "Improvement in Microstructure Homogeneity of Sintered Compacts through Powder Treatments and Alloy Designs", Materials Science Forum, Vols. 534-536, pp. 537-540, 2007

Online since:

January 2007




[1] K. S. Hwang, C. H. Hsieh, and G. J. Shu: Powder Metall. Vol. 45, No. 2 (2002), p.160.

[2] L. Zhang, Z-Y Li, K-C Zhou, and F Liu: Mat. Sci. and Eng. Powder Metall. Vol. 10, No. 4 (2005), p.225.

[3] K.S. Hwang and M.Y. Shiau: Metall. and Mat. Trans., Vol. 27B (1996), p.203.

[4] H. Zhang and R. M. German: Int. J. Powder Metall. Vol. 38, No. 1 (2002), p.51.

[5] S. T. Campbell, T. Singh, and F. Stephenson: Adv. in P/M and Particulate Materials, Part 7 (2004), MPIF, Princeton, NJ, p.105.

[6] A. L. Sozinov and V. G. Gavrilijuk: Scripta Mater. Vol. 41, No. 6 (1999), p.679.

[7] M. W Wu, K. S. Hwang, and K. S. Narasimhan: submitted to Mat. and Metall. Trans. 50μm 50μm 50μm 50μm.