Mechanical and Microwave Dielectric Properties of Csf/Si3N4 Composites


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Csf/Si3N4 composites were prepared by hot-press sintering method using α-Si3N4 power, short chopping carbon-fiber and sintering additives. XRD analysis showed that the α-Si3N4 was almost completely transferred into β-Si3N4. The SEM micrographs of fractured surfaces showed that special network developed by rod-like β- Si3N4 grains. The flexure strength of 590±10MPa, and fracture toughness of 7.94±0.1MPa·m1/2 were achieved for the samples incorporated with 0.5wt% the carbon fibers .The microwave dielectric property of Csf/Si3N4 composites was measured at a frequency range of 8.2~18GHz by E8362B PNA series network analyzer. The real part (ε ′ ) of the permittivity of the Csf/Si3N4 composites increases from 10 to 58 with the rise of the content of carbon fibers in the composites, as well as the imaginary part increases from 0.03 to 98 at frequency of 9.375GHz. A strong frequency dependence of the real part was observed both in X and Ku bands.



Materials Science Forum (Volumes 546-549)

Edited by:

Yafang Han et al.




X. Y. Wang et al., "Mechanical and Microwave Dielectric Properties of Csf/Si3N4 Composites", Materials Science Forum, Vols. 546-549, pp. 1661-1664, 2007

Online since:

May 2007




[1] R. N. Katz and R. B. Schulz: Nitrogen Ceramics, Martinus Nijhoff Publishers, (1983), pp.727-36.

[2] R. Hamminger and J. Heinrich: MRS Proceedings, vol. 287(1993), pp.513-520.

[3] Cs Bala' zsi., F.S. Cinar, O. Addemir, F We' ber., P. Arato': Journal of the European Ceramic Society, vol. 24(2004), pp.3287-3294.


[4] N. Hirosaki, Y. Akimune, and M. Mitomo: J. Am. Ceram. Soc., 76.

[7] (1993), pp.1892-94.

[5] Y. Goto and A. Tsuge: J. Am. Ceram. Soc. 76.

[6] (1993), pp.1420-24.

[6] Z. Shen, Z. Zhao, H. Peng and M. Nygren: Nature, vol . 417(2002), pp.266-269.

[7] Thompson, D. P.: Nature, vol. 417, 237(2002).

[8] B. Derby: Cur. Op. Solid State Mat. Sci. vol. 3(1998), pp.490-495.

[9] E. Naeumann, K. Rebstock, H.G. Riedel, K.H. Roess, S. Wolfsried, U.S. Patent No. 6302246(2001).

[10] PS. Bradshaw.: Proceeding of SAMPE. Amsterdam; (1989), pp.187-196.

[11] J. H. Oh, K. S. Oh, C. G. Kim, C.S. Hong: Compos Part B(2004), pp.49-56.

[12] R Schueler, Petermann J, Schulte K, Wentzel HP: J Appl Polym Sci vol. 63(1997), pp.1741-6.

[13] Heinrich J. Rocker E et al: J. Am. Ceram. Soc., vol. 71(1)(1988), p. C -28.

[14] Akhlesh Lakhtadia, Bernhard Michel, Werner S Weiglhofe: J. Phys. D: Appl. Phys. Vol. 30(1997), pp.230-240.