Microstructure Evolution during Warm Deformation of Low Carbon Steel with Dispersed Cementite


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The microstructure evolution and mechanical behavior during large strain of a 0.16%CMn steel has been investigated by warm torsion tests. These experiments were carried out at 685 °C at equivalent strain rate of 0.1 s-1. The initial microstructure composed of a martensite matrix with uniformly dispersed fine cementite particles was attained by quenching and tempering. The microstructure evolution during tempering and straining was performed through interrupted tests. As the material was reheated to testing temperature, well-defined cell structure was created and subgrains within lath martensite were observed by TEM; strong recovery took place, decreasing the dislocation density. After 1 hour at the test temperature and without straining, EBSD technique showed the formation of new grains. The flow stress curves measured had a peculiar shape: rapid work hardening to a hump, followed by an extensive flow-softening region. 65% of the boundaries observed in the sample strained to ε = 1.0 were high angle grain boundaries. After straining to ε = 5.0, average ferrite grain size close to 1.5 1m was found, suggesting that dynamic recrystallization took place. Also, two sets of cementite particles were observed: large particles aligned with straining direction and smaller particles more uniformly dispersed. The fragmentation or grain subdivision that occurred during reheating and tempering time was essential for the formation of ultrafine grained microstructure.



Materials Science Forum (Volumes 558-559)

Edited by:

S.-J.L. Kang, M.Y. Huh, N.M. Hwang, H. Homma, K. Ushioda and Y. Ikuhara




J. Gallego et al., "Microstructure Evolution during Warm Deformation of Low Carbon Steel with Dispersed Cementite", Materials Science Forum, Vols. 558-559, pp. 505-510, 2007

Online since:

October 2007




[1] R.Z. Valiev, R.K. Islamgaliev and I.V. Alexandrov: Prog. Mater. Sci. Vol. 45 (2000), p.103.

[2] Y. Saito, H. Utsunomiya, N. Tsuji and T. Sakai: Acta Mater. Vol. 49 (1999), p.579.

[3] Z. Horita, D. Smith, M. Furukawa, M. Nemoto, R.Z. Valiev, T.G. Langdon: J. Mater. Res. Vol. 11 (1996), p.1880.

[4] T. Inoue, S. Torizuka and K. Nagai: International symposium on ultrafine grained steels (ISUGS 2001), Fukuoka, Japan. The Iron and Steel Institute of Japan (2001), p.88.

[4] S. Takaki, K. Kawasaki and Y. Kimura: J. Mater. Proc. Techon. Vol. 117 (2001), p.359.

[5] P.J. Hurley and P.D. Hodgson: Mater. Sci. Eng. Vol. A302 (2001), p.206.

[6] A. Najafi-Zadeh, J.J. Jonas and S. Yue: Metal. Trans. Vol. 23A (1992), P. 2607.

[7] R. Ueji, N. Tsuji, Y. Minamino and Y. Koizumi: Acta Mater. Vol. 50 (2002), p.4177.

[8] A. Ohmori, S. Torizuka and K. Nagai: ISIJ Inter. Vol. 44 (2004), p.1063.

[9] G. A. Redfern and C. M. Sellars: Jounal of The Iron and Steel Institute, June 1970, p.576.

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