Papers by Author: Feng Zhou

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Authors: An Min Hu, Kai Ming Liang, Feng Zhou, Fei Peng, Guoliang Wang
Abstract: The mechanical properties of spodumene-diopside glasses ceramics with 4-12% TiO2 were investigated. The main crystalline phases precipitated were eucryptite, β-spodumene and diopside. As TiO2 content increasing, the morphology of glass ceramics transformed from coarse to fine microstructure, then to reverse. The flexural strength, elastic moduli, Vickers hardness and fracture toughness of the glass-ceramics were measured. The flexural strength of glass–ceramics containing 9%TiO2 was 198MPa, the Young’s modulus and fracture toughness were 91.3GPa and 2.3 MPa·m1/2 respectively. It was indicated that the mechanical properties were correlated with crystallization and morphology of glass ceramics
1639
Authors: Hua Shao, Kai Ming Liang, Feng Zhou, Fei Peng
Abstract: Crystallization sequence of MgO-Al2O3-SiO2-TiO2 system glass was investigated by means of DTA, XRD, SEM and EDS. The relationship between crystalline phases, heat treatment methods and thermal expansion coefficient (α) were well discussed. The results have shown that: The glass first underwent extensive phase separation into titanium-rich droplets in a silica-rich matrix, then magnesium aluminotitanate (MAT) initially precipitated in the droplet phases. With the crystallization temperature increased, β-quartzss, sapphirine, α-quartzss and α-cordierite made their appearance successively. The thermal expansion coefficient as a function of the heat treatment condition was studied.
1635
Authors: Feng Zhou, Ying Qing Fu, Kai Ming Liang
Abstract: The crystallization behavior and microstructure of Li+-doped TiO2 thin films prepared by sol-gel dip coating were investigated by means of differential themal analysis (DTA), X-ray diffraction (XRD) and scanning electron microscopy (SEM). The crystallization apparent activation energy (E) both in the absence and in the presence of Li+ ion was also measured with Kissinger method. As a result the E values of Li+-doped TiO2 thin film were decreased, thus the crystallization of non-crystalline to anatase and antase to rutile was promoted.
750
Authors: Shu Ming Wang, Kai Ming Liang, Le Fu Mei, Feng Zhou
Abstract: The effect of Fe2O3-TiO2 mixture additives on the crystallization behaviour of a parent glass with composition located in the primary field of cordierite within the MgO-Al2O3-SiO2 system has been examined. The crystallization behaviour of the glass was determined by differential thermal analysis (DTA) and X-ray diffraction (XRD). The microstructure was characterized by scanning electron microscopy (SEM). The results show that additives of Fe2O3-TiO2 can lower the temperature of the crystallization peak (Tp) and promote crystallization of the parent glass. By controlled thermal treatment, the main crystal phase obtained was Fe2+substituted α-cordierite. The approach outlined in this paper to obtain heterogeneous ion substituted cordierite glass-ceramics is useful to develop infrared radiation material with good properties.
1856
Authors: Guoliang Wang, Kai Ming Liang, Wei Liu, An Min Hu, Feng Zhou, Hua Shao
Abstract: By means of SEM, the micro-morphology of silver particles separated from borosilicate glass by the heat-treatment with an electric field is investigated. The distribution of the silver particles appears clusters. This result is explained by an energy viewpoint. Based on hermodynamics theory of phase separation, the calculation of the free energy change during the heat-treatment in an electric field is performed by means of the Ansoft Maxwell software. The results of this calculation analysis are found to be very close to the experimental data.
1647
Authors: Fei Peng, Kai Ming Liang, Hua Shao, An Min Hu, Feng Zhou
Abstract: The nucleation and crystallization kinetics of glass obtained by melting coal fly ash with additives at 1550°C have been investigated. The optimum heat treatment schedule for the glass was nucleation at 825°C for 60min before crystallization at 962°C for 4h. The activation energy for crystallization of the glass-ceramics, obtained by the DDTA result, was 280.03 kJ/mol, lower than that of glass-ceramics obtained from pure reagents. The low activation energy is caused by impurities in fly ash, serving as nucleation agent. The results of XRD and SEM show that glass-ceramics developed nano-sized spherical wollastonite.
1651
Authors: Le Fu Mei, Kai Ming Liang, Shu Ming Wang, Feng Zhou
Abstract: ZrO2-TiO2 thin films, which were heat-treated with an applied electric field, were prepared by sol-gel method. The phase transformation behavior of ZrO2-TiO2 composite thin films was studied by DTA, XRD, SEM and Raman spectroscopy. In an electric field, the phase transformation temperature of amorphous phase to anatase and that of anatase to rutile are all decreased.
2316
Authors: Feng Zhou, Ying Qing Fu, Xin Wan
Abstract: A facile route was demonstrated to obtain an efficient graphene-hybridized TiO2 photocatalyst. The photodegradation results of Methylene Blue over graphene hybridized with TiO2 showed that the photocatalytic activity could be significantly enhanced under UV light irradiation. The structure between TiO2 and graphene as well as its effect on the photocatalytic activity were systematically investigated. The mechanism of the enhanced photocatalytic activity is based to the high migration efficiency and the inhibition of recombination of photoinduced electron-hole pairs. The graphene hydridization is proven to be a promising approach to develop highly efficient and stable photocatalysts under UV light irradiation.
1677
Authors: Feng Zhou, Kai Ming Liang, Hua Shao, An Min Hu
Abstract: LiNO3-doped TiO2 thin films on glass-ceramics were prepared by sol-gel dip coating. The influence of LiNO3 addition on the phase transformation temperature was studied. The transformation temperatures of non-crystalline to anatase and anatase to rutile are originally 520°C and 880°C without the addition of LiNO3. By adding 5%LiNO3 the two transformation temperatures decrease to 440°C and 580°C, respectively. The average size of the particles was found to be around 40nm for the LiNO3- doped TiO2 film annealed at 600°C.
805
Authors: Feng Zhou, Hui Chen Zhang, Kai Ming Liang
Abstract: In this paper the Li+, Sb3+-doped SiO2-TiO2 thin films, which were heat-treated with an applied electric field, were prepared by sol-gel dip coating. The crystallization of the thin films in the electric field heating-treatment was studied by X-ray diffraction (XRD) and atomic force microscope (AFM). The photo-catalytic activity of SiO2-TiO2 films was studied under the condition of an electric field heating-treatment and mixing with some additive such as Li+ and Sb3+. Finally, studies on photo-catalytic degradation showed that the Li+, Sb3+-doped SiO2-TiO2 films on the quartz glass, of high photo-catalytic activity, were successfully obtained in the electric field heating-treatment.
1865
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