Papers by Author: Jian Bao Li

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Authors: Hong Lin, Ning Wang, Xiao Zhan Yang, Jian Bao Li
Abstract: In this paper, firstly, titanate nanotubes was synthesized by hydrothermal method with commercial antase-type TiO2 powder as the raw material. TiO2 nanotubes (TNTs) can be obtained by heat-treating the as-prepared titanate nanotubes at 400 °C. Secondly, an electrode with 30 % TNTs and 70% nanocrystalline TiO2 was designed and prepared successfully. By using the nano-electrode as the photoanode of DSC, the light-to-energy conversion efficiency of 5.42 % was obtained. In addition, the effect of hydrothermal temperature on the crystal growth of nanotubes and the effect of tert-butyl pyridine (TBP) on the photoelectric performance of the DSC were also discussed.
Authors: Fa Hui Li, Jian Bao Li, Hong Lin, Cun Xin Huang, Mu Yun Lei, Hong Bing Du
Abstract: The present paper summarizes the technology and basic process for fabricating transparent ceramic MgAl2O4 spinel and introduces a scalable production technique. Fully transparent polycrystalline spinel has been prepared by combined vacuum sintering, hot-pressing, sintering in H2 atmosphere and hot isostatic pressing(HIP). The optical transmittance of the specimen sintered at 1500°C following HIP at 1800°C was nearly the same as that of single crystal spinel. When radiated by γ-ray and X- ray, colorless spinel became brown due to V-type color centers, which decreased its transmittance. On the other hand, the spinel ceramics’ resistance to radiation improved by doping CeO2.
Authors: Jing Zhang, Hong Lin, Jian Bao Li, Xin Li, Xiao Chong Zhao
Abstract: Screen printing has been considered to be the simplest and quickest way to fabricate dye- sensitized solar cells (DSCs) modules for an assembly line. 20cm×10cm DSCs modules with W-type series connection and parallel connection were fabricated. The whole fabricating process was all operated by screen-printing except for the injection of electrolyte. The optimized TiO2 electrode thickness, sealant thickness and platinum counter electrode thickness were investigated. The modules showed a reliable performance.
Authors: Ning Wang, Xiao Zhan Yang, Jian Bao Li, Hong Lin, Bo Chi
Abstract: Mullite powders of stoichiometric composition were synthesized by sol-gel process with TEOS and Al(NO3)3·9H2O as silicon and aluminum source. Homogeneous mullite powders were used as the starting materials to prepare the porous mullite coating on the porous silicon carbide support by repeated dip-coating method. XRD analysis revealed that the mullite precursor gels almost completely transformed to orthorhombic crystalline mullite at 1200°C. The average pore diameter and porosity of the porous mullite coating were about 4.5µm and 52.3%, respectively.
Authors: Junichi Matsushita, S. Yasumatsu, N. Hosaka, K. Okawa, T. Fujita, Jian Bao Li, Hong Lin, Kwang Bo Shim
Abstract: The fabrication and fluorescence properties of luminescence porous ceramics were investigated by using recycling glass addition of oxide phosphor to determine the suitability of this material for the application of recycling glass. The aim of this study was to give the fluorescence performance to the porous ceramics using recycling glass with phosphor material. The samples showed a good "Eco" luminescence porous ceramics of about 60 to 70 % porosity using recycling glass.
Authors: Gang Feng Guo, Xiao Zhan Yang, Jian Bao Li, Hong Lin, Long Liang, Ming Sheng He, Xu Guang Tong
Abstract: Silicon nitride ceramics were fabricated with Yb2O3 as the sintering additive. The effects of the amount of Yb2O3 on the microstructure and the mechanical properties such as the flexural strength and the fracture toughness were investigated. Almost fully densified Si3N4 was obtained when only 4 wt% Yb2O3 was added. Both the flexural strength and the fracture toughness increased steadily with the Yb2O3 content. The transgranular fracture mode was observed in the specimen containing 4 wt% Yb2O3, however, the intergranular fracture mode was observed in the specimen containing 10 wt% Yb2O3.
Authors: Xin Gang Yu, Lan Yun Liu, Yan Bin Zuo, Zhi Peng Xie, Bo Lin Wu, Jin Long Yang, Jian Bao Li, Yong Huang, Lin Wang, Yi Gong
Abstract: A heated sprue device for ceramic injection moulding was used to research the defects in injection-moulded technical ceramics. By use of the heated sprue device, the problem of sprue solidification was resolved and the density of the injection moulding specimens was increased while the defects eliminated. The influence of the processing parameters on the defects of the injection molding specimens was investigated in detail by X-ray radiography camera and photograph. It turns that the sprue solidification time has much influence on the defects in injection-moulded technical ceramics. Reasons causing the results above were also analyzed. Based on the research, bars of 20mm in diameter without macroscopic defects and turbine blade of fine property with Si3N4/SiC(w) materials were prepared by injection moulding.
Authors: Xu Guang Tong, Xiao Zhan Yang, Jian Bao Li, Geliang Sun
Abstract: In this paper, the models of multilayer absorbing coating and hollow ball are studied. For the former model, a computer program is made to simulate absorbing results with the electromagnetic transmission line theory. The results show that there is a relevant absorbing peak at different frequencies for different dielectric constant (ε) and the apex’s height and position change with ε and thickness of the multilayer coatings. This program can predict the coating’s absorbing property efficiently. With the latter model, it is found that SiC hollow micro-balls whose porosity is about 0.89 make the best absorbing effect.
Authors: Xu Guang Tong, Jian Bao Li, Hong Lin, Xiao Zhan Yang, Jun Yang
Abstract: The effects of rare earth oxides (Lu2O3 and La2O3) on the property, microstructure and oxidation behavior of hot-pressing sintered Si3N4 ceramics were investigated. The silicon nitride ceramics with Lu2O3 and La2O3 as addition have been fabricated by hot-pressed at 1800°C for 1h under a pressure of 25MPa. Oxidation test was carried out at 1400°C in air for 100 hours. Mechanical properties, SEM and XRD were measured before and after oxidation. The results showed that Si3N4 ceramics doped Lu2O3 had good microstructure and mechanical properties than those doped La2O3. Oxidation test showed a parabolic weight gain with oxidation time at 1400°C in air and the oxidation products of the ceramics were SiO2, Re2Si2O7 and Re2SiO5 confirmed by XRD and EDS. The rate-controlling step was the diffusion of ion. The samples doped Lu2O3 showed superior oxidation resistance to those doped La2O3.
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