Papers by Author: Kai Ming Liang

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Authors: Shuang Xi Wang, Kai Ming Liang, Xiao Hui Zhang, Hai Bin Li, Shou Ren Gu
745
Authors: Bing Yu, Kai Ming Liang, Pei Sheng Liu, Shou Ren Gu
449
Authors: An Min Hu, Kai Ming Liang, Feng Zhou, Fei Peng, Guoliang Wang
Abstract: The mechanical properties of spodumene-diopside glasses ceramics with 4-12% TiO2 were investigated. The main crystalline phases precipitated were eucryptite, β-spodumene and diopside. As TiO2 content increasing, the morphology of glass ceramics transformed from coarse to fine microstructure, then to reverse. The flexural strength, elastic moduli, Vickers hardness and fracture toughness of the glass-ceramics were measured. The flexural strength of glass–ceramics containing 9%TiO2 was 198MPa, the Young’s modulus and fracture toughness were 91.3GPa and 2.3 MPa·m1/2 respectively. It was indicated that the mechanical properties were correlated with crystallization and morphology of glass ceramics
1639
Authors: Hua Shao, Kai Ming Liang, Feng Zhou, Fei Peng
Abstract: Crystallization sequence of MgO-Al2O3-SiO2-TiO2 system glass was investigated by means of DTA, XRD, SEM and EDS. The relationship between crystalline phases, heat treatment methods and thermal expansion coefficient (α) were well discussed. The results have shown that: The glass first underwent extensive phase separation into titanium-rich droplets in a silica-rich matrix, then magnesium aluminotitanate (MAT) initially precipitated in the droplet phases. With the crystallization temperature increased, β-quartzss, sapphirine, α-quartzss and α-cordierite made their appearance successively. The thermal expansion coefficient as a function of the heat treatment condition was studied.
1635
Authors: Le Fu Mei, Kai Ming Liang
Abstract: The Mg-doped TiO2 was prepared by Sol-gel method at low temperature. The crystallization of TiO2 was studied by DTA, it was shown that the phase transition temperature of the Mg (NO3)2-doped TiO2 from amorphous to anatase and then to rutile significantly reduce. The XRD results show that the Mg-doped TiO2 has anatase and rutile annealed at 600 °C. Studies of photo-catalytic degradation show that the photo-catalytic activity of Mg-doped TiO2 thin film is higher than that of non-doped TiO2.
847
Authors: Feng Zhou, Ying Qing Fu, Kai Ming Liang
Abstract: The crystallization behavior and microstructure of Li+-doped TiO2 thin films prepared by sol-gel dip coating were investigated by means of differential themal analysis (DTA), X-ray diffraction (XRD) and scanning electron microscopy (SEM). The crystallization apparent activation energy (E) both in the absence and in the presence of Li+ ion was also measured with Kissinger method. As a result the E values of Li+-doped TiO2 thin film were decreased, thus the crystallization of non-crystalline to anatase and antase to rutile was promoted.
750
Authors: Shu Ming Wang, Kai Ming Liang, Le Fu Mei, Feng Zhou
Abstract: The effect of Fe2O3-TiO2 mixture additives on the crystallization behaviour of a parent glass with composition located in the primary field of cordierite within the MgO-Al2O3-SiO2 system has been examined. The crystallization behaviour of the glass was determined by differential thermal analysis (DTA) and X-ray diffraction (XRD). The microstructure was characterized by scanning electron microscopy (SEM). The results show that additives of Fe2O3-TiO2 can lower the temperature of the crystallization peak (Tp) and promote crystallization of the parent glass. By controlled thermal treatment, the main crystal phase obtained was Fe2+substituted α-cordierite. The approach outlined in this paper to obtain heterogeneous ion substituted cordierite glass-ceramics is useful to develop infrared radiation material with good properties.
1856
Authors: Guoliang Wang, Kai Ming Liang, Wei Liu, An Min Hu, Feng Zhou, Hua Shao
Abstract: By means of SEM, the micro-morphology of silver particles separated from borosilicate glass by the heat-treatment with an electric field is investigated. The distribution of the silver particles appears clusters. This result is explained by an energy viewpoint. Based on hermodynamics theory of phase separation, the calculation of the free energy change during the heat-treatment in an electric field is performed by means of the Ansoft Maxwell software. The results of this calculation analysis are found to be very close to the experimental data.
1647
Authors: Fei Peng, Kai Ming Liang, Hua Shao, An Min Hu, Feng Zhou
Abstract: The nucleation and crystallization kinetics of glass obtained by melting coal fly ash with additives at 1550°C have been investigated. The optimum heat treatment schedule for the glass was nucleation at 825°C for 60min before crystallization at 962°C for 4h. The activation energy for crystallization of the glass-ceramics, obtained by the DDTA result, was 280.03 kJ/mol, lower than that of glass-ceramics obtained from pure reagents. The low activation energy is caused by impurities in fly ash, serving as nucleation agent. The results of XRD and SEM show that glass-ceramics developed nano-sized spherical wollastonite.
1651
Authors: Le Fu Mei, Kai Ming Liang, Shu Ming Wang, Feng Zhou
Abstract: ZrO2-TiO2 thin films, which were heat-treated with an applied electric field, were prepared by sol-gel method. The phase transformation behavior of ZrO2-TiO2 composite thin films was studied by DTA, XRD, SEM and Raman spectroscopy. In an electric field, the phase transformation temperature of amorphous phase to anatase and that of anatase to rutile are all decreased.
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