Papers by Keyword: Grain Boundary Migration

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Authors: Tatiana Gorkaya, Thomas Burlet, Dmitri A. Molodov, Günter Gottstein
Abstract: A novel set-up developed to continuously observe and measure stress driven grain boundary migration is presented. A commercially available tensile/compression SEM unit was utilized for in-situ observations of mechanically loaded samples at elevated temperatures up to 850°C by recording orientation contrast images of bicrystal surfaces. Two sample holders for application of a shear stress to the boundary in bicrystals of different geometry were designed and fabricated. The results of first measurements are presented.
819
Authors: Yan Huang
Abstract: Solute drag theory is critically revisited and an alternative approach is presented to account for the effect of solute elements on grain boundary migration during annealing. A fundamental new concept is introduced in the model that, in the linear range of irreversible thermodynamics, solute atoms segregated in a grain boundary will not lag behind when the boundary migrates. While lagging behind is the very essential assumption for the solute drag theory. Instead of blaming the lagging behind, the mobility drop due to solute addition is attributed to the decrease in boundary energy as a result of boundary segregation. According to this model, grain boundary mobility is dependent on solute concentration rather than migration rate. The predictions of the model are compared with experimental results, with a good agreement.
131
Authors: Dmitri A. Molodov, U. Czubayko, Günter Gottstein, Lasar S. Shvindlerman
1493
Authors: Sandra Piazolo, David J. Prior, M.D. Holness, Andreas O. Harstad
Abstract: Annealing is an important mechanism of microstructural modification both in rocks and metals. In order to relate directly changes in crystallographic orientation to migrating boundaries the researcher has the option to investigate either samples where the grain boundary motion can be directly tracked or a series of samples exhibiting successively higher degrees of annealing. Here we present results from rock samples collected from two well characterised contact aureoles (a volume of rock heated by the intrusion of a melt in its vicinity): One quartz sample in which patterns revealed by Cathodoluminescence (CL) indicate the movement of grain boundaries and a series of calcite samples of known temperature history. Electron backscatter diffraction (EBSD) analysis is used to link the movement of grain, twin boundaries and substructures with the crystallographic orientation / misorientation of a respective boundary. Results from the quartz bearing rock show: (a) propagation of substructures and twin boundaries in swept areas both parallel and at an angle to the growth direction, (b) development of slightly different crystallographic orientations and new twin boundaries at both the growth interfaces and within the swept area, and (c) a gradual change in crystallographic orientation in the direction of growth. Observations are compatible with a growth mechanism where single atoms are attached and detached both at random and at preferential sites i.e. crystallographically controlled sites or kinks in boundary ledges. Strain fields caused by defects and/or trace element incorporation may facilitate nucleation sites for new crystallographic orientations at distinct growth interfaces but also at continuously migrating boundaries. Calcite samples show with increasing duration and temperature of annealing: (a) systematic decrease of the relative frequency of low angle grain boundaries (gbs), (b) decrease in lattice distortion within grains, (c) development of distinct subgrains with little internal lattice distortion, (d) change in lobateness of gbs and frequency of facet parallel gbs and (e) change in position of second phase particles. These observations point to an increasing influence of grain boundary anisotropy with increasing annealing temperature, while at the same time the influence of second phase particles and subtle driving-force variations decrease. This study illustrates the usefulness of using samples from natural laboratories and combining different analysis techniques in microprocess analysis.
333
Authors: A. Suzuki, Yuri M. Mishin
Abstract: We present results of atomistic computer simulations of spontaneous and stress-induced grain boundary (GB) migration in copper. Several symmetrical tilt GBs have been studied using the embedded-atom method and molecular dynamics. The GBs are observed to spontaneously migrate in a random manner. This spontaneous GB motion is always accompanied by relative translations of the grains parallel to the GB plane. Furthermore, external shear stresses applied parallel to the GB and normal to the tilt axis induce GB migration. Strong coupling is observed between the normal GB velocity vn and the grain translation rate v||. The mechanism of GB motion is established to be local lattice rotation within the GB core that does not involve any GB diffusion or sliding. The coupling constant between vn and v|| predicted within a simple geometric model accurately matches the molecular dynamics observations.
157
Authors: Suk Joong L. Kang
Abstract: This paper reviews our recent investigations on grain growth in ceramics. Grain growth behavior has been found to be governed by the grain boundary structure: normal growth with a stationary relative grain size distribution for rough boundaries and non-normal (nonstationary) growth for faceted boundaries. Based on the concept of nonlinear migration of faceted boundaries, the mixed control model of grain growth is introduced and the principle of microstructural evolution is deduced. This principle states that various types of grain growth behavior are predicted as a result of the coupling effect between the maximum driving force for growth and the critical driving force for appreciable migration of the boundary. A wealth of experimental results supports the theoretical predictions of grain growth behavior, showing the generality of the suggested principle of microstructural evolution. Application of this principle is also demonstrated for the fabrication of single crystals as well as polycrystals with desired microstructures.
377
Authors: A. Katsman, Leonid Klinger, L. Levin, Eugen Rabkin, W. Gust
493
Authors: Duk Yong Yoon
193
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