Structural and Magnetic Properties of Chemically Deposited Hexaferrites

Article Preview

Abstract:

M-type lead hexaferrites (PbFe12O19) have been prepared using sol-gel methods. Lead and iron precursors were dissolved in butoxyethanol and stabilised with acetylacetone to produce a sol with good wetting and surface coating characteristics. Powder samples were investigated to optimise conditions for the growth of thin films. The «spin on» technique was used to provide homogeneous films. X-ray diffraction and thermomagnetic analysis vibrating sample magnetometry have been performed to assess phase distribution and transformation. The results show that the hexaferrite phase can be crystallised above 700 °C and that for the first indication that this phase is metastable in air below 650 °C.

You might also be interested in these eBooks

Info:

Periodical:

Materials Science Forum (Volumes 514-516)

Pages:

304-308

Citation:

Online since:

May 2006

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2006 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] Oliver, S. A., Yoon, S. D., Kozulin, I., Chen, M. L. & Vittoria, C., Growth and characterization of thick oriented barium hexaferrite films on MgO (111) substrates, Appl. Phys. Lett., 2000, 76, 3612-3614.

DOI: 10.1063/1.126723

Google Scholar

[2] Qi, X. W., Zhou, J., Yue, Z. X., Gui, Z. L. & Li, L. T., Study on magnetic and dielectric properties of ferroelectric/ferromagnetic composites, Electronic Components & Materials, 2003, 22, 3-5.

Google Scholar

[3] Díaz-Castañón, S., Leccabue, F., Watts, B. E., Yapp, R., Asenjo, A. & Vázquez, M., Oriented PbFe12O19 thin films prepared by pulsed laser deposition on sapphire substrate, Mater. Lett., 2001, 47, 356-361.

DOI: 10.1016/s0167-577x(00)00266-4

Google Scholar

[4] Chiorboli, G., Leccabue, F., Watts, B. E., Di Cristoforo, A., Mengucci, P. & Majni, G., The crystallisation behaviour of Pb(ZrTi)O3 sol-gel films on platinum electrodes, Mat. Sci. and Eng B, 1997, 47, 263-268.

DOI: 10.1016/s0921-5107(97)00044-5

Google Scholar