Authors: J.C. Outeiro, A. Morão Dias
Abstract: Machining residual stresses are considered as part of surface integrity and a consequence
of the machining process. Theses stresses are closely correlated with the corresponding process
parameters, including the work material properties. As it is well known, not only the mechanical but
also the physical properties of the work materials have great influence on machining residual stress.
This was demonstrated in the present work through studying the residual stress and work hardening
induced by the turning of AISI 316L and AISI 1045 steels. The residual stresses were determined at
the workpiece surface and in-depth using the X-ray diffraction technique. To understand the
influence of the work material properties on the residual stress and work hardening distributions, the
mechanical and thermal phenomena occurring during the cutting process were studied, using a t
developed experimental procedure. The experimental setup included a piezoelectric dynamometer to
determine the cutting forces, and thermal imaging equipment developed to assess the temperature
distribution in the deformation zone in turning. The results showed that the cutting forces and
temperatures in the machining of 316L steel are much higher than those in the machining of 1045
steel. Thus, machining 316L steel, when compared to 1045 steel, results in higher superficial
residual stresses and stronger in-depth residual stress gradients, higher superficial work-hardening
and greater thickness of the work hardened layer.
575
Authors: Maria José Marques, J.C.P. Pina, A. Morão Dias
Abstract: The conventional Bragg diffraction geometry, normally used to characterize the residual
surface stress state, it is not suitable to evaluate surface treated materials and thin films. The X-ray
path lengths through a surface layer or thin film are too short to produce adequate diffraction
intensities in relation to the bulk or the substrate. Another limitation of the conventional technique
appears when a residual stress gradient is present in the irradiated surface. The technique only
enables the evaluation of the mean value of this gradient. In these cases, a recently proposed
Pseudo-Grazing Incident X-ray Diffraction method would be better applicable.
In this study, the Pseudo-Grazing Incidence X-ray Diffraction is applied to characterize the residual
stress depth profiles of several AISI 4140 samples, which were prepared, by mechanical polishing
and grinding, in order to present different surface roughness parameters, Ra. The experimental
results lead to the conclusion that the surface roughness limits the application of the
Pseudo-Grazing Incidence methodology to a minimum X-ray incident angle. This angle is the one
that enables a mean X-ray penetration depth with the same order of magnitude of the sample surface
roughness parameter, Ra.
1618
Authors: J.C.P. Pina, Maria José Marques, J.M.M. dos Santos, A. Morão Dias
Abstract: The thin and textured coatings present a double difficulty for characterization by
conventional X-ray diffraction. Their shallow depth reduces the diffracted intensity and allows the
interference of the underlying material. Frequently they present a crystallographic texture which
limits the number of orientations that provide good intensity and induces anisotropy effects on their
mechanical behavior. Reliable results can be determined using diffraction geometry of lowincidence
angle. This paper describes the application of the technique to several films, characterized
by thicknesses of the order of 1 μm and crystallographic textures. Examples are proposed of
chromium films applied by PVD on molybdenum substrates, decorative electroplated coatings, and
aluminum coatings used for interconnections in microelectronic circuits. The Cr films are 1.5 μm
thick and exhibit a strong <100> fiber texture. The decorative coatings were studied both on the
nickel undercoat and in the Cr top layer. Results are presented for chromium where tensile stresses
and a <110> fiber texture were observed. The Al films are 1.0 μm thick. Some samples were heattreated
at different annealing temperatures. Tensile stresses were always observed, which increase in
the annealed samples.
1613
Authors: António Castanhola Batista, Joao P. Nobre, A. Morão Dias
Abstract: A characterisation technique based on the stress determination by X-ray diffraction has
been developed. It enables the identification of elastoplastic stress-strain laws on materials
presenting an in-depth gradient of mechanical properties on its cross section. This technique is
especially suitable to the characterisation of surfaces due to the small X-rays penetration depth. The
method was applied in the characterisation of a carbonitrided and shot-peened steel, allowing to
evaluate the stress-strain laws of the material at the surface, the intermediate layers and the bulk
material. In addition, the in-depth evolution of microhardness, residual stresses, diffraction peak
broadening and retained austenite contents were analysed. This allowed to understand the results of
the proposed technique.
1623
Authors: Joao P. Nobre, Altino Loureiro, António Castanhola Batista, A. Morão Dias
Abstract: In this work the reliability of the hole-drilling technique (HDT) for measuring welding residual stresses was analysed. HDT residual stress results were systematically compared with those determined by X-ray diffraction. A systematic overestimation of the residual stresses determined by HDT was observed, which was mainly attributed to the possibility of the so-called plasticity effect occurring. Experimental results were discussed taking the measurement principles of both
techniques into consideration. In addition, preliminary results of a numerical study, using the finite element method, will be presented for a better understanding of the plasticity effect on HDT residual stress results.
768
Authors: António Castanhola Batista, José P. Marinheiro, Joao P. Nobre, A. Morão Dias
Abstract: An inverse method for the characterisation of the elastoplastic behaviour of materials has been studied. The method is based on spherical indentation test data and numerical analysis of the indentation process, enabling to find a characteristic stress-strain curve. This method will be appropriate for elastoplastic behaviour study, mainly on surface hardened materials, when the standard methods cannot be applied. In this work, the method was applied to annealed and quenched steels, with homogeneous properties over the cross section. The obtained results are in
good agreement with those obtained from the standard tensile tests. However, if the material does not follow a linear hardening law, the elastoplastic characteristics determined by the inverse method will depend on the indentation depth. For these cases a method for the evaluation of the actual behaviour law has been improved.
744
Authors: Maria José Marques, J.C. Outeiro, A. Morão Dias, Rachid M'Saoubi, Hariharan Chandrasekaran
Abstract: The quality of a mechanical component such as its geometrical accuracy stability and
fatigue life are significantly affected by the surface integrity generated by machining process. Residual stresses are a major part of the mechanical state of a machined layer and they can be beneficial or detrimental depending of their nature and magnitude. This study concerns phase analysis and residual stress profile characterization by X-ray diffraction (XRD) technique and microhardness profile of AISI H13 ESR mould steel, milled using carbide and CBN tools.
Analysis of the cross-section of the AISI H13 ESR samples, milled using both tools, reveal a martensitic microstructure, with a very thin layer heavily deformed due to the machining process. However, no phase transformation was detected by XRD.
Concerning the residual stresses, the results show that they are predominantly compressive at the samples surface. However, depending of the cutting tools, the in-depth residual stresses profiles present different evolutions. This difference in the in-depth residual stresses profiles between the two kind of cutting tools is attributed to the different cutting tool parameters, including the tool geometry.
564
Authors: P. Matos, Pedro Miguel Guimarães Pires Moreira, J.C.P. Pina, A. Morão Dias, Paulo Manuel Salgado Tavares de Castro
Abstract: Cold working introduces a compressive stress field around rivet holes, reducing the
tendency for fatigue cracks to initiate and grow under cyclic mechanical loading. As it is well known, for the accurate assessment of fatigue lifetimes a detailed knowledge of the residual stress profile is required. Powerful experimental and numerical tools are nowadays available for that purpose. In the present work both types of tools, X-ray diffraction and 3D Finite Element Analysis (FEA), were used
in order to evaluate the residual stress profile. A comparison of experimental and numerical data is presented and discussed.
41
Authors: Joao P. Nobre, U. Noster, Martin Kornmeier, A. Morão Dias, Berthold Scholtes
267
Authors: Maria José Marques, A. Morão Dias, C. Gautier-Picard, Jean Lu Lebrun
152