Papers by Author: Feng Lei Huang

Abstract: Different TiO2 precursors were impacted by detonation-driven high velocity flyers to obtain high-pressure phases of titania under instantaneous high temperature and pressure. The factors affecting high-pressure phase synthesis such as loading conditions and titanium dioxide precursors were also studied. The structure and phase composition of the shocked samples are determined by X-ray diffraction (XRD). The microstructure of TiO2 after shock treatment was observed by transmission electron microscopy (TEM).

Abstract: In this paper, nitrogen-doped titania was achieved by detonation-driven flyer impacting on the mixtures of TiO2 and different nitrogen precursors. XRD、UV-Vis and XPS spectra were employed to characterize the phase composition, N doping concentration and energy gap of recovered samples. N doping concentration can be effectively regulated by choosing different doping nitrogen resources, changing initial content of doping nitrogen resources and flyer velocity in order to regulate the energy gap of TiO2. The maximum concentration of nitrogen of doped TiO2 by shock loading at 3.37 km/s is 13.45 at%. The results show that anatase transforms to rutile and srilankite appears at a higher flyer velocity (1.9-2.52km/s), the concentration of doped nitrogen in the recovered samples increases with increasing flyer velocity, the maximum concentration of nitrogen is 13.45 at%. The edge adsorption wavelength of nitrogen-doped titania induced by shock wave is shifted from 435nm to 730 nm and the corresponding energy gap is reduced from 2.85 eV to 1.73 eV.

Abstract: The spider silk is considered as a new type of biomaterials with its excellent mechanical properties. The mechanical properties of the spider silk are crucial to their applications. In this study the mechanical properties of spider silk were studied with a micro-tensile system driven by magnet-coil force actuator, which is very effective to measure the properties of low dimensional materials. The Young’s modulus of the spider silk is obtained, the relationship between the mechanical properties of spider silk and time is also acquired.

Abstract: Creep properties of polymer bonded explosives (PBXs), a particulate composite, was studied by using the method of moiré interferometry in this paper. The specimens fabricated by different heat pressing technology were used. Extensive creep deformation of PBXs material was indirectly measured by the aid of compressive circular disk test. The obtained results shown that creep properties are greatly influenced by pressing pressures and temperature of heat pressing technology. The results indicated that the higher the temperature and the pressing pressure are in the heat pressing technology to some degree, the better the PBXs material creep resistance is. The creep fracture surfaces of PBXs were also observed using Scanning Electronic Microscopy (SEM). It was shown that most of the fracture crack was initiated and propagated along the explosives crystal surface during creep.

Abstract: Martensitic phase transformation can greatly affect the mechanical behaviors and the stress-strain response of shape memory alloys (SMAs). In this study, the effect of martensitic phase transformation on the deformation of a single-crystal TiNi SMA specimen with a triangle crack was investigated experimentally by means of moiré interferometry method. A typical displacement field and the corresponding strain field in areas both around and far from the tip of the crack were measured in a certain time during the loading process in which the tensile load is coupled with the stress-induced martensitic phase transformation. Some characteristics of the deformation and the martensitic phase transformation of the specimen are revealed. These results may provide a reliable support for revealing the fracture mechanism of single crystal TiNi SMAs, and may enable further development in putting forward the failure criterion of SMAs.

Abstract: In this study, the digital image correlation method(with Newton-Raphson iteration method) is used to measure the in-plane deformation of poly-crystal aluminum. When the specimen is exerted a tensile load, the strain distribution of the specimen surface will be inhomogeneous. The micro-deformation of the poly-crystal aluminum is studied under a SEM(scanning electron microscope), a series of images of the micro crystal are captured during the loading process. By using digital image correlation to analyze the images, the displacement and strain of a micro-crystal are obtained, which provide important data for further analysis of the inhomogeneous properties of the poly-crystal aluminum.

Abstract: In this paper, a novel nano-moiré grating fabrication technique was proposed for nanometer deformation measurement. The grating fabrication process was performed with the aid of Atomic Force Microscope (AFM) on the basis of micro-fabrication technique. On the analysis of some correlative factors of influencing grating line quality, some important experimental parameters were optimized. In this study, some parallel and cross nano-gratings with frequencies of from 10000lines/mm to 20000lines/mm were fabricated. The successful experimental results demonstrate that the nano-grating fabrication technique is feasible and also indicated that these nano-gratings with nano-moiré method can be applied to deformation measurement, which offers a nanometer sensitivity and spatial resolution.

Abstract: In this paper, the creep deformation of PBX was measured using the moiré interferometry. The experimental results show a different creep process compared with pure high polymer and this phenomenon is preliminary analyzed from damage mechanics.