Papers by Author: Fu Min Xu

Abstract: Electron beam melting is an effective method to remove volatile impurities in silicon, during which impurities such as P, Al and Ca etc. can be removed to less than 0.3×10^-4wt.%. However, so far there is few research on the influence of electron beam parameters, such as beam density and beam size, on molten pool morphology, hence electron beam melting process has not been completely understood, which leads to low energy utilization. In this paper, on the basis of beam size calibration, the influence of beam density and beam size on molten pool morphology is investigated and the concept of melting angle is proposed to characterize molten pool morphology. At the same time, the optimal molten pool morphology for impurities removal and the corresponding electron beam parameters are also analyzed.

Abstract: Five-layered Al/Al-Cu functionally graded material (FGM) was fabricated by powder metallurgy technology. The microstructure and composition of the prepared specimen were studied. Vickers hardness, flexural strength and fracture surface morphology were also measured. The results showed that Al/Al-Cu graded material with dense structure and compositional continuous change was obtained by solution-precipitation method. The graded materials presented a compositional continuous change along the graded direction because of the diffusion effect, and the Vickers hardness was liner proportional to the distribution of Cu content. Compared with pure sintered Al, remarkable improvement on hardness and fracture strength was achieved due to the CuAl2 phase dispersively distributed in the matrix. With the increase of Cu content, the fracture mode changed from tough fracture to the tendency of brittle fracture.

Abstract: AlN ceramics were prepared by hot-pressing process with Y(NO3)3·6H2O as a sintering additive. Microstructure and mechanical properties of sintered AlN ceramics were measured and compared with that of monolithic AlN ceramic prepared by the same process. The results showed that the density and mechanical properties of monolithic AlN ceramics were drastically enhanced by adding Y(NO3)3·6H2O. Especially, the AlN ceramic with 3.24 wt% Y(NO3)3·6H2O (2 wt% Y2O3) displayed striking enhancement in mechanical propertie. However, such enhancement did not follow a consistent behavior with the increase of Y(NO3)3·6H2O content. A significant drop present at contents over inflection point (3.24 wt% Y(NO3)3·6H2O).

Abstract: Effect of heat treatment in atmosphere on the resistivity of polycrystalline silicon has been investigated in this paper. After heat treatment at 1050oC for 10h, there is no obvious change of the resistivity in the N-type region of polycrystalline silicon, which could be contributed to the complicated influence factors, such as more impurities content and defects. On the other hand, an obvious increase of the resistivity was observed in the P-type region which could be contributed the redistribution of Al and B in the Si-SiO2 interface. The resistivity of the P-type region increased from less than 1Ω·cm to several hundreds Ω·cm.

Abstract: The distribution of resistivity, impurity and polarity in multicrystalline silicon ingot prepared by directional solidification method was detected. The effect of impurity distribution on resistivity was also researched. The results show that the shapes of equivalence line of resistivity in the cross section and vertical section of the silicon ingot depend on the solid-liquid interface. The resistivity in the vertical section increases with the increasing of solidified height at the beginning of solidification and reaches to maximum at the polarity transition point, then decreases rapidly with the increasing of solidified height and tends to zero on the top of the ingot because of the high impurity concentration. Study proves that the variation of resistivity in the vertical section is mainly relevant to the concentration distribution of the impurities such as Al, B and P in the growth direction.