Papers by Author: M. Abo-Elsoud

Abstract: High-energy ball-milling in hexane medium was employed to prepare Nobel Zr-based bulk metallic glasses (BMGs) alloy of three different nominal compositions Zr47Be23Ni15Ti15, Zr50Be20Ni15Ti15 and Zr52Be18Ni15Ti15, numbers indicate at.%). The glass forming ability was found to increase with decreasing Zr and increasing Be content, which can be ascribed to the enhanced atomic size mismatch of the constituents on Be addition. Amorphous Zr47Be23Ni15Ti15 powder undergoes two-stage crystallization with onset temperatures at 640 and 700 K and glass transition temperature Tg at 566 K. In contrast, the Zr50Be20Ni15Ti15 and Zr52Be18Ni15Ti15 samples remained crystalline to a certain extent even after prolonged milling and contained FCC Zr crystallites. Structural characterization was done by X-ray diffraction (XRD) and transmission electron microscopy (TEM). In addition, thermal analyses were performed by means of differential scanning calorimetry (DSC) thermogram to justify the experimental findings.

Abstract: SEM observations and Vickers-hardness tests were performed to identify the irradiation effects. γ- irradiation effect during the aging hardening process can be explained depending on the composition of the alloy and is used to derive quantitative information on the kinetics of the transformation precipitates. Increasing the Cu content of an Al-Cu alloy can improve the aging hardness. The present results of hardness behavior with SEM observations of surveillance specimens at different doses suggest that the radiation-induced defects are probably complex valance-solute clusters. These clusters act as nuclei for the precipitation of θ-Al2Cu type. This can be effectively utilized to study the systematic of nucleation of precipitates at vacancy-type defects. γ-irradiation probably play the key role in defects responsible for material strengthening and embrittlement.

Abstract: Micro-structural change caused by the corresponding change in creep properties of Cu-8.5at.%Al alloy was studied. It was found that a micro-structural observations reveal the formation of different types of defect features during creep of the investigated alloy at intermediate temperatures between 0.46-0.72Tm, where Tm is the absolute melting point. SEM was used to characterize the studied alloy by quantitative micro-analysis. It allowed the observer to defect the micro-structural features such as dislocation that were generated from deformation and could move interagranularly by glide and climb. Clearly, the development of this microstructure could be attributed to the grain refining effect of the Al indicating the role of the applied stress at this alloy. The results show that the creep rupture strength of Cu-8.5at.%Al alloy in the power law creep damage mechanism. This due to the constraint introduced on the matrix creep flow by the Al phase rather than the devolvement of high threshold stress values. While the increase in the length of Al filaments and reduction in interfilament spacing with increasing draw ratio increase the constraint on the creep flow of the matrix, they also enhance the creep damage caused by the diffusion mechanisms because of the easy diffusion paths along the Al filaments and the reduction in the matrix grain size.

Abstract: Creep experiments were conducted on Cu-8.5at.% Al alloy in the intermediate temperature range from 673 to 873K, corresponding to 0.46-0.72 Tm where Tm is the absolute melting temperature. The present analysis reveals the presence of two distinct deformation regions (climb and viscous glide) in the plot of log ε vs. log σ. The implications of these results on the transition from powerlaw to exponential creep regime are examined. The results indicated that the rate controlling mechanism for creep is the obstacle-controlled dislocation glide. A phenomenological model is proposed which assumes that cell boundaries with sub-grains act as sources and obstacles to gliding dislocations.

Abstract: Positron Annihilation Doppler Broadening Spectroscopy (PADPS) is one of the nuclear techniques used in material science. PADPS measurements are used to study the behavior of defect concentration and dislocation density in a set of 3003 and 3005 wrought aluminum alloy. It has been shown that positrons can become trapped at imperfect locations in solids. The S-parameter can be influenced by changes in the concentration of such defects. There is no observed change in the Sparameter values after the saturation of defect concentration. The S-parameter and trapping rates for the samples deformed up to 10 percent were studied. The concentration of defect range varies from 1017 to 1018 cm-3 and from 1016 to 1017 cm-3 for 3003 and 3005 wrought Al alloy respectively. While trapping rate range varies from 1 x1010 to 1.2x1011 s-1 for 3003 and from 1 x109 to 1.2x1010 s-1 for 3005 wrought Al alloy.