Papers by Author: Sang Ll Lee

Abstract: The long-term corrosion resistances for the carbon steels have been investigated under high temperature pressurized water atmosphere, in the conjunction with the analysis of nondestructive properties by the ultrasonic wave. The corrosion test for carbon steels was carried out at the temperature of 200 °C under a water pressure of 10 MPa. The corrosion test cycles for carbon steels were changed up to 65 weeks. The mechanical properties of carbon steel suffered from the corrosion cycle were investigated by a tensile test, attaching an acoustic emission sensor on the test sample. The tensile strength of carbon steels greatly decreased beyond the corrosion cycle of 35 weeks, accompanying the increase of weight loss by the creation of corrosion damages. The attenuation coefficient of carbon steels by the ultrasonic wave increased with the increase of corrosion cycles.

Abstract: A study on corrosion evaluation by using ultrasonic waves and acoustic emission technique is presented. The experimental equipment was established to improve the corrosion process of carbon steel pipe. The carbon steel pipe was under 473K temperatures and 10Mpa pressure conditions, and ultrasonic wave and acoustic emission techniques were used to inspect the degree of corrosion after a certain period of time. Ultrasonic bulk waves are limited by the poor time resolution when used in the measurement of corrosion depth in thin wall structures because the corroded surfaces cause unclear echo signal edges. Therefore, in this study, the ultrasonic guided waves were generated on the pipe because the thickness of pipe was thin. Various wave modes were subsequently generated on the pipe to evaluate the implications of corrosion thinning on group velocity, transmission and reflection amplitudes. The amplitudes of the transmitted and the reflected waves are influenced by couplent material. In order to reduce the effect of coupling acoustic emission sensor was used. Acoustic emission technique has lots of parameters to evaluate the corrosion besides amplitude parameter. Among parameters energy, count, and frequency were useful parameters to measure the degree of corrosion inside the carbon steel pipe under 473K temperatures.

Abstract: The nuclear power plant has lots of pipes that the fluid of high temperature and high pressure flows. Among the pipe materials used at secondary circuit of the power plant the carbon steels are sensitive to corrosion due to their material properties. In this study, both ultrasonic test and acoustic emission test were used to study the corrosion effect for the carbon steel pipe nondestructively. The carbon steel specimens were in the pipe under 473K temperatures and 10MPa pressure conditions for corrosion processing. According to the degree of corrosion the strength of the specimen was evaluated, and the thickness of the corrosion specimens was also measured by using the ultrasonic wave. The experimental results showed that the attenuation factor was also increased as a depth of corrosion increased. The measured depth of the real corrosion by ultrasonic test shows the good agreement with that by an optical microscope. In order to understand the corrosion effect for the failure mechanism of carbon steel, a failure test on the specimen with various corrosion conditions was performed. An acoustic emission technique was also used to evaluate the degree of damage of corrosion specimen in real time. Acoustic emission technique is proved a useful method for on-line monitoring the microscopic failure mechanism and the damage location for the structures.

Abstract: This study dealt with the corrosion resistance for the carbon steels under a pressurized water atmosphere at the elevated temperature. The nondestructive test was also used to evaluate the damage degree of corrosion test specimen. The corrosion test for carbon steels was carried out at the temperature of 200 °C under a water pressure of 10 MPa. The corrosion time for carbon steel was changed up to 20 weeks. The strength of carbon steel by the degree of corrosion was investigated by a tensile test. The carbon steel showed an average tensile strength of about 500 MPa after the corrosion period of 20 weeks, accompanying the weight loss of about 2.5 %. The attenuation coefficient of ultrasonic wave can be utilized as useful parameters to inspect the corrosion damages of carbon steels.

Abstract: Copper/aluminum/stainless steel (Cu/Al/STS) clad materials were made by rolling and heat treatment process. These specimens were evaluated the formability and bonding strength of Cu/Al/STS clad materials. Thin disc specimens for TEM observation were prepared from the interfaces of Cu/Al and Al/STS by using the Focused Ion Beam (FIB) utility. Brittle oxide film formed on copper surface during heat treatment at 673K~773K. Diffusion bonding was observed at the interface of Cu/Al. Reacted region was formed in the interface of Al/STS with width about 10nm, while in the case of Cu/Al was formed about 1,600nm width. It was also observed nanosized crevice in reacted region of Al/STS interfaces.

Abstract: In this study, elastic waves of ultrasonic and acoustic emission were used to evaluate the propagation characteristic of the wave in pipe, and study on mode conversion of the elastic wave due to the cracks in the pipe was also performed. An acoustic emission (AE) sensor was used to receive the propagated ultrasonic wave. AE technique has a merit that it can identify the received ultrasonic wave by the analysis of the AE parameters such as count, energy, frequency, duration time and amplitude. For transmitting and receiving of the wave, a wedge for universal angle was manufactured. The optimum angles for transmitting of ultrasonic wave and signal receiving at the attached AE sensor on the pipe were determined. Theoretical dispersion curve was compared with the results of the time-frequency analysis based on the wavelet transformation. The received modes showed a good agreement with theoretical one. The used ultrasonic sensor was 1MHz, and AE sensor was broadband (100kHz – 1200kHz). The artificial cracks were induced in the pipe to measure the propagation characteristics of the elastic wave for the cracks. AE parameters for the received signals were also varied with the crack types in the pipe. AE parameters of amplitude and duration time were more effective factors than the analysis of mode conversion for evaluation of the cracks in the pipe.

Abstract: The long-term corrosion strength properties for the carbon steels under pressurized water atmosphere have been investigated, in the conjunction with the detailed analysis of their microstructures. The corrosion test for carbon steels was carried out at the temperature of 200°C under a water pressure of 10 MPa. The corrosion test samples were maintained up to 50 weeks in the tube shaped reactor. The mechanical strength and the microstucture of carbon steels suffered from the long term corrosion test were evaluated by SEM, XRD and tensile test. The weight loss of carbon steel by the corrosion test was also examined. The tensile strength of carbon steels decreased with the increase of corrosion time under a pressurized water atmosphere, accompanying the creation of severe corrosion damages like stress corrosion crack.

Abstract: The objective of this paper is to investigate the applicability of ultrasonic wave technique to monitor the progress of the thermal shock damage on alumina ceramic. For this purpose, alumina ceramic specimen was heated in the furnace and then was quenched into the water tank. The initiation, growth behaviors of surface micro-cracks as a function of the number of thermal shock cycle have been discussed by taking into account the change of ultrasonic wave velocity and attenuation. The change of both velocity and attenuation of ultrasonic wave showed good relation with the surface crack density changing due to the number of thermal shock cycle. Measuring the change of attenuation gives more effective information to evaluate thermal shock damage than that of velocity nondestructively. The flexural strength was also measured for the thermal shocked specimen. The flexural strength was decreased rapidly at the point of time of observation of microcracks on the surface of specimen, and the flexural strength decline by the crack growth caused thermal shock cycles was slight.

Abstract: This paper dealt with the fabricating process of liquid phase sintered (LPS) SiC ceramics containing the oxide additives of Al2O3 and Y2O3, in conjunction with the evaluation of their mechanical properties. LPS-SiC ceramics was sintered at the temperature of 1820 oC under an applied pressure of 20 MPa and a pressure holding time of 2 hour. A commercial SiC powder with an average size of about 0.3 μm was used as a starting powder. LPS-SiC ceramics with additive composition ratios of 1.5 and 2.3 (Al2O3/Y2O3) represented an excellent density of about 3.2 Mg/m3. LPS-SiC ceramics had a flexural strength of about 800 MPa and a fracture toughness of about 8.0 MPa⋅m0.5 at an additive composition ratio (Al2O3/Y2O3) of 1.5.

Abstract: A new type of thermotropic main-chain liquid crystalline polyurethanes containing biphenyl units was synthesized by polyaddition reaction of diisocyanates such as 2,6-tolylene diisocyanate, 2,5-tolylene diisocyanate, 2,4-tolylene diisocyanate, and 1,4-phenylene diisocyanate, with 4,4′-Bis(11-hydroxyundeyloxy)biphenyl (BP11). The structure of the monomer and the corresponding polymers were confirmed FT-IR and 1H NMR spectroscopic methods. BP11 exhibited a smectic type mesophase, however, nematic phase was found for all synthesized liquid crystalline polyurethanes except for 1,4-phenylene diisocyanate/BP11 based polyurethane. For example, polyurethane 2,5-TDI/BP11 exhibited monotropic liquid crystallinity in the temperature ranges from 173 to 156 °C on the cooling stage.