Authors: T. Akita, Masahide Gotoh, Sergey V. Dobatkin, Kazuo Kitagawa, Yukio Hirose
Abstract: In the present study, ultra fine-grained low carbon steel samples were processed by equal channel angular pressing (ECAP). Mechanical properties of the specimens annealed statically at several temperatures were evaluated by tensile and hardness test. In addition, grain sizes of the specimens were measured by SEM-electron back scattering pattern (SEM-EBSP) and X-ray diffraction analysis. Differential scanning calorimetry (DSC) measurement also evaluated thermal reactions in anneal process of the specimen. As a result, the grain size was changed at the temperature between 550oC and 600oC drastically and the tensile strength also became lower at the same temperature. The relation between yield stress and averaged grain diameter of specimens obeyed the Hall-Petch relation except the normalized specimen. Behavior of grain growth and recovery in structural observation by EBSP corresponded to reaction signal of the DSC curve.
1899
Authors: Hung Wei Yen, Chi Yuan Huang, Jer Ren Yang
Abstract: The ferrite phase strengthened by the highly dense nanometer-sized carbides is named super ferrite. The effects of Ti, Ti-Mo, and Ti-Nb micro-alloy additions on the precipitation strengthening in three experimental high-strength low-alloy steels have been investigated by using transmission electron microscopy and micro-hardness measurement. The objective of this work was to study the carbide precipitation under the conditions of isothermal transformation. It was found that interphase precipitation of nano-sized carbide in Steel Ti-Mo had very strong contribution to the hardness of the steel. The distribution of interphase precipitated carbides is associated with both the sheet spacing and the inter-particle spacing, which have been studied. The result implies that (Ti, Mo)C particles possess an excellent effect on precipitation hardening.
663
Authors: Mohammad Badaruddin, Chaur Jeng Wang
Abstract: Low carbon steel was coated by hot-dipping into a molten Al-10%Si bath. The high-temperature oxidation was performed at 700oC for 1 h to 49 h in air, air +100% H2O, and air + 30% ethanol under atmospheric pressure. An elemental composition distribution, morphologies of the aluminide layer and the oxide scale were characterized by OM, XRD, and SEM/EDS. After hot-dipping treatment, the coating layers consisted of Al, Si, FeAl3, τ5-Fe2Al8Si, and Fe2Al5. The results of high temperature oxidation tests showed the oxidation rate were parabolic law in three different atmospheres. The polyhedral τ1-(Al,Si)5Fe3 formed at a short time oxidation completely transformed to FeAl2 and FeAl due to the composition gradient and the chemical diffusion. The effect of water vapor on the oxidation resistance of the Al-Si coating may be attributed to increase in Al and Fe ions transport, leading to loss of protective aluminide layer by formation of iron oxide nodules on the coating surface and at interface between aluminide layer and the steel substrate.
1775
Authors: Hui Shu Zhang, Dong Ping Zhan, Song Lian Bai, Zhou Hua Jiang
Abstract: The corrosion behaviors of Al-Si-Cr-Cu bearing low carbon steel and a reference steel Q235 were tested in a cyclic dry/wet environment containing 0.01mol/L NaHSO3 in laboratory. Rust layers were observed by optical microscope (OM), scanning electron microscopy (SEM) and XRD. The electrochemical behaviors of the steels were studied on the polarization curves and electrochemical impedance spectroscopy (EIS). The results indicate that after 120h corrosion test, the annual corrosion rates of the designed steels reduce 42 % than Q235 at least. The corrosion products are generally iron oxyhydroxides and oxides such as FeOOH, γ-FeOOH, α-FeOOH, γ-Fe2O3, Fe3O4. The α-FeOOH possesses good stabilization mainly exits and can improve the corrosion resistance. There are the enrichments of Cu, Cr, Si and Al in the rust layer close to the matrix, which make the rust layer be more compact and protected. The corrosion currents of the two designed steels are lower than that of Q235, the corrosion potentials are higher than that of Q235 after Tafel fitting. The rust layer impedances of the designed steels are higher than that of Q235.
1017
Authors: Jiang Hua Ma, Dong Ping Zhan, Zhou Hua Jiang, Ji Cheng He
Abstract: In order to understand the effects of deoxidizer such as aluminium, titanium and magnesium on the impact toughness of heat affected zone (HAZ), three low carbon steels deoxidized by Ti-Al, Mg and Ti-Mg were obtained. After smelting, forging, rolling and welding simulation, the effects of Al, Ti and Mg addition on the impact toughness of HAZ in low carbon steel were studied. The inclusion characteristics (size, morphology and chemistry) of samples before welding and the fracture pattern of the specimens after the Charpy-type test were respectively analyzed using optical microscope and scanning electron microscopy (SEM). The following results were found. The density of inclusion in Ti-Mg deoxidized steel is bigger than Ti-Al deoxidized steel. The average diameter is decreased for the former than the latter. The addition of Ti-Mg can enhance the impact toughness of the HAZ after welding simulation. The maximal value of the impact toughness is 66.5J/cm2. The complex particles of MgO-TiOx-SiO2-MnS are most benefit to enhance impact toughness. The improvement of HAZ is attributable to the role of particle pinning and the formation of intergranular ferrite.
143
Authors: Hai Bo Xie, Zheng Yi Jiang, Yan Bing Du, Dong Bin Wei, A. Kiet Tieu
Abstract: Surface roughness plays an important role in determining the tribological behaviour of mechanical components (e.g. gears and roller bearings etc.) under full-film and mixed (or partial) elastohydrodynamic lubrication conditions. This paper describes a detailed mechanics analysis of the surface roughness transformation of thin strip which has been cold rolled on an experimental mill. Low carbon steel strips were rolled at various speeds and reductions, and the effects of rolling parameters on surface roughness are studied. The results of surface roughness can provide important information to optimise the rolling schedule and to improve the rolled strip quality.
544
Authors: Elena G. Astafurova, Sergey V. Dobatkin, Evgeny V. Naydenkin, Svetlana V. Shagalina, Galina G. Zakharova
Abstract: Ultrafine grained low carbon steel processed by high pressure torsion (HPT) has been
investigated. Depending on initial state (ferritic-pearlitic state after normalization at 950°C, or
martensitic ones after quenching from 950°C and 1180°C), the evolution of the microstructure and
the mechanical properties was investigated after HPT and annealing at 400-600°C using
transmission electron microscopy and X-ray analysis. It has been shown that HPT of martensitic low
carbon steel provides a finer structure then that for ferritic-pearlitic initial state, and the initial
martensitic morphology and phase composition is strongly dependent on the temperature of
quenching. The initial structure was refined by HPT to 95nm in ferritic-pearlitic state and up to 65
and 50 nm in martensitic ones (after quenching from 950°C and 1180°C, respectively). Such
ultrafine grained structures demonstrate substantial mechanical properties and possess a high
thermal stability up to 500°C in all investigated states. Annealing for 1 h at 500°C results in grain
growth up to 860nm for ferritic-pearlitic initial state and 150-450 nm for martensitic ones.
649
Authors: Sergey V. Dobatkin, P.D. Odessky, Svetlana V. Shagalina
Abstract: The structure, mechanical and functional properties of ultrafine-grained low-carbon steels
have been studied after severe plastic deformation (SPD) by high pressure torsion (HPT) and equalchannel
angular pressing (ECAP). It is revealed that HPT of low carbon steels at a temperature
below 0.3 Tm leads to the formation of nanocrystalline structure with a grain size of <100 nm or a
mixture of oriented substructure and nanograins. ECAP under similar conditions leads to the
formation of submicrocrystalline structure with a grain size of 200-300 nm. The initial martensitic
state compared with the initial ferritic-pearlitic state of the low-carbon steels results in formation of
finer structure after SPD and less intense grain growth upon heating, i.e., results in a higher thermal
stability. Low-carbon low-alloy steels after ECAP are characterized by high strength (UTS > 1000
MPa) and plasticity (EL = 10-15%). The high-strength state after ECAP is retained upon tensile test
testing up to a temperature of 500°C. The submicrocrystalline low-carbon steels after ECAP
processing and subsequent heating is characterized by an increased impact toughness at test
temperatures down to -40°C.
623
Authors: Hitoshi Ozaki, Reiji Ichioka, Takashi Matsuura, Muneharu Kutsuna
Abstract: Titanium is one of structural materials. It has several advantages such as high corrosion
resistance and high strength-to-weight ratio. The demand of titanium structural panel and the
dissimilar joint has been increased in industry. It is well known that joining of steel and titanium is
difficult because of generating the brittle intermetallic compound. In the present work, the laser roll
welding of dissimilar metals, titanium to low carbon steel been investigated using a 2.4kW CO2
laser and a 2kW fiber laser. The effects of process parameters on the formation of intermetallic
compound at the interlayer and on the mechanical properties were investigated to get a sound
dissimilar metal joint. As a result, welded joints of titanium to low carbon steel were broken in the
base metal of low carbon steel in the tensile-shear test.
543
Authors: Kyohei Kawamoto, Yasuji Oda, Hiroshi Noguchi
Abstract: In order to investigate the hydrogen effect on fatigue crack growth (FCG) behavior in a few
kinds of practical alloys; austenitic stainless steels (solution-treated metastable type 304 and stable
type 316L), an aluminum alloy (age-hardened 6061) and a low carbon steel (annealed 0.13%C-Fe),
FCG tests were carried out in hydrogen gas and in nitrogen gas. The FCG rates of these materials are
enhanced by hydrogen, though the acceleration degrees are different. A crack grows across grains by
slip-off in 316L stainless steel and in age-hardened 6061 aluminum alloys even in hydrogen. Faceted
area increases in 304 stainless steel and in low carbon steel in hydrogen. In 304 stainless steel, the
ratio of facets to the entire fracture surface was not so large. Thus, the FCG rate is not significantly
affected through the facets in 304 stainless steel. In low carbon steel, facets were increased
considerably, though a crack grows step by step or after a large number of loading cycles even along
grain boundaries. Anyhow hydrogen enhances the FCG rate of these materials through the influence
on slip behavior. Based on above-mentioned results, the effect of loading frequency on FCG rate in
hydrogen of the age-hardened 6061 aluminum alloy was also investigated. The FCG rate increases as
the testing frequency decreases, though the FCG rate in hydrogen shows the tendency to saturate.
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