Papers by Keyword: Martensite Phase

Abstract: The main purpose of this investigation was to study the effect of strain hardening on wear properties of 316 austenitic stainless steel (ASS). Cold deformation was performed by using a universal tensile machine for 20% CW and 40% CW followed by heat treatment to relieve internal stresses. A secondary cold working process was performed for the heat-treated samples followed by a secondary heat treatment. Wear test measurements and microscopic examinations were preformed for all samples. It was observed that by increasing the strain hardening percentage the hard brittle martensite phase increases. Also, by increasing both the SiC grit of the emery papers (which was used in the wear test) and the time of the wear test, the weight lost per unit area was decreased. The wear resistance was increased by using single and double 20% strain hardening but by exceeding the cold working to more than 40% the wear resistance decreased.

Abstract: Beta stabilizing elements cause high processing cost due to their high density and high melting point. Ti-xMo-2Fe alloy is metastable beta titanium alloy containing a low-cost beta stabilizing elements, and it is possible to secure excellent price competitiveness. Microstructure characterization and mechanical properties of a new designed Ti-xMo-2Fe alloys were investigated by Optical microscope, Vickers hardness, room temperature tensile test, in this study. The microstructure and mechanical properties were different depending on Mo contents, and Ti-9.2Mo-2Fe showed high hardness and brittle failure due to the high Mo content. As a result, Ti-3.4Mo-2Fe showed a tensile strength of 821.2 MPa and a high elongation of 10.3%.

Abstract: Polarisation methods, and Open circuit potential measurements have been utilized to evaluate the impact of heat remediation on the corrosion characteristics of CuAlNi shape memory alloy in 3.5 percent NaCl solutions. CuAlNi alloy specimens were investigated in their as-sintered condition and following a thermal remediation processing that included annealing at 900 °C for 60 min associated with water quenching, and 200-degree centigrade for 30 hrs. and rapid cooling in iced water. The enhancement in polarisation resistance and reduction in corrosion rate of heat-treated CuAlNi alloy further suggests that heat remediation has a positive effect on CuAlNi alloy corrosion resistance. After measurements of polarisation, optical microscopy, SEM/EDX, and XRD examination of specimen surfaces reveal the presence of corrosion damage on the electrode surfaces, with CuCl2, AlCl3, and Cu2Cl (OH)3 compounds as surface corrosion products..

Abstract: Recently, biomaterial α + β type Ti alloys with relatively low Young’s modulus and high specific strength have been widely used all over the world. Martensite (M) phase in α + β type Ti alloy has been reported to improve the toughness and ductility, therefore, there is high possibility of improvement in the mechanical properties easily by controlling the volume fraction of M phase. In this study, the change in mechanical properties of α + β type Ti-6Al-7Nb (Ti67) with various volume fractions of M phase were systematically investigated through the various heat treatments and thermo-mechanical treatments. Microstructures of Ti67 subjected to ST at 1173 K to 1273 K below the temperature of β transus were composed of martensite and primary α phases. The volume fraction of M phase increased with an increase in ST temperature. Tensile strength increased simply with an increase in the volume fraction of M phase, while the elongation, reduction of area and Young’s modulus showed a reverse trend. Fatigue limit of Ti67 subjected to ST at 1243K showed the highest value of 880 MPa.

Abstract: The effects of nickel content and heat treatment conditions on the creep strength of precipitation-strengthened 15Cr ferritic steel were investigated. The creep strength of the 15Cr ferritic steel was drastically improved by solution treatment and water quenching. However, over the long term, the detrimental effect of nickel on the creep strength was pronounced for water-quenched steels. The volume fraction of martensite phase increased with increased nickel content in both the furnace-cooled and water-quenched steels. The volume fraction of martensite phase in the water-quenched steel was smaller than that in the furnace-cooled type, even for the same nickel content. Fine particles, smaller than 500 nm, were precipitated homogeneously within the ferrite phase of the water-quenched steel. On the other hand, coarse block-like particles 1 $m in size were precipitated sparsely within the martensite phase. The creep strength of the steels decreased with increased volume fraction of the martensite phase caused by furnace cooling and nickel addition. The lower creep strength and microstructural stability of the martensite phase is attributable to less precipitation strengthening. To enable this steel to be put to practical use, it will be necessary to suppress the formation of the martensite phase caused by addition of nickel by optimizing the chemical composition and heat treatment conditions.

Abstract: The system free energy was estimated for the martensite phase of an Fe-Cr-C ternary alloy, 12Cr2W and 12Cr2W0.5Re steels. The system free energy of the martensite phase is defined as, Gsys = G0 + Estr + Esurf , where G0 is the chemical free energy, Esurf is the interfacial energy for the boundaries in the martensite microstructure, and Estr is the elastic strain energy due to the dislocations in the martensite phase. From the experimental results on SEM/EBSD, the total interfacial energies were estimated to be 0.83J/mol for the ternary alloy and 4.8J/mol for both 12Cr2W and 12Cr2W0.5Re steels in the as-quenched state. Also, the elastic strain energies were estimated to be 7.1J/mol for the ternary alloy, 9.6J/mol for 12Cr2W steel and 9.8J/mol for 12Cr2W0.5Re steel in the as-quenched state. So, the system free energy was about 7.9J/mol for ternary alloy. On the other hand, the system free energy was about 14.4J/mol for 12Cr2W steel and 14.6J/mol for 12Cr2W0.5Re steel. So, these microstructural energies operate as a driving force for the microstructure evolution, e.g., recovery of dislocations and the coarsening of the sub-structures such as martensite-packet, -block and -lath.