Papers by Keyword: Microtexture

Abstract: The development of orientation spreads within individual grains of a polycrystal submitted to large deformations is analysed by both experiment and simulation. In the experiment, 176 grains on an internal surface of a split sample were followed by detailed EBSD measurements, at successive strains up to 1.2. In parallel, a high-resolution finite element simulation has been carried out on the same polycrystal configuration. For both experiment and simulation, hundreds to thousands of orientation values were obtained in each grain. Most grains showed a “unimodal” rotation, composed of an average rotation and an orientation spread. The experimental and simulated orientation spreads were compared through different statistical metrics. The average lattice disorientations are found to increase rapidly at the beginning of the deformation and to saturate at high strains. The orientation spreads are also analysed in terms of anisotropy along the sample axes. It is shown that the orientation spreads are aligned preferably along TD at the beginning of the deformation, then tend to move to RD in the experiment, and RD or ND in the simulation.

Abstract: We elaborated two carbide-free bainitic steels with different microstructures through specific heat treatments and alloy design. EBSD analysis was used to point out major differences in these microstructures. In-situ characterizations of the bainitic transformation were performed by high energy synchrotron diffraction to go further into the study of each phase characteristics. The elaborated microstructures exhibited various phase fractions of bainitic ferrite, retained austenite and blocks of martensite and retained austenite. Moreover, the volume fraction of retained austenite increased with higher austempering temperatures. On the other hand, the austempering temperatures showed a strong influence on the kinetics of the bainitic transformation. Isothermal transformation under Ms showed a two stage transformation which led first to the formation of self-tempered martensite and then to bainitic ferrite. Furthermore, the evolution of the austenitic cell parameter showed enrichment in carbon ruled by diffusional mechanisms.

Abstract: The mechanism responsible for the formation of recrystallization texture is still disputed although recrystallization texture has long been a subject of research. This is mainly related to the complexity of recrystallization itself .The mechanism of recrystallization microtexture Cold-rolling low carbon sheet steel based on CSP was investigated by the electron back scatter diffraction(EBSD) was investigated. In addition, the origin of nuclei with specific orientations was studied. The results showed that the formation of recrystallization texture is explained by oriented nucleation and the nucleis show around 50% frequency of 15–60°misorientation with their surrounding deformed matrices. Deformed γ-fibre texture components increase more rapidly during the early stage of recrystallization. In contrast, the deformed α-fibre components, such as {001}<110> components disappear rather rapidly early stage of recrystallization and {112}<110> components increases rapidly late stage of recrystallization and grains growth. By microcosmic orientation distribution analyse find that the new {011}<100> grains are nucleated within shear bands in the deformed {111}<112> grains, New {111}<112> grains are nucleated within deformed {111}<110> grains and new {111}<110> grains originated in the deformed {111}<112> grains .

Abstract: This paper describes microstructure and microtexture development in dissimilar friction welded -TAB-Ti64 joints. The effect of friction welding parameters on microstructure and local properties are examined and discussed. It was found that the intermetallic -TiAl based alloy Ti-47Al-3.5(Mn+Cr+Nb)-0.8(B+Si) (denoted as -TAB) is more sensitive to the applied friction welding parameters used in this study. Furthermore, the bonding between these two alloys was controlled by a diffusion process during a very short process duration. Grain refinement as well microstructure transformation led to local improvement of the friction-welded joints.

Abstract: The texture and microstructure resulting from heavily drawn and annealed oxygen-free high conducting (OFHC) copper wires have been investigated using several microscopical techniques including orientation imaging microscopy and nano-indentation. In the as-drawn condition, the microstructure and texture were heterogeneous across the wires, and consisted of three distinct concentric regimes: the inner core, the mid section, and the outer region. Whilst the microtexture of the inner core was dominated by a strong <111>+weak<100> duplex fiber texture, the mid section and the outer region had a comparatively weak fiber texture. Analysis using a Taylor-type viscoplasticity model revealed that the weak texture observed in this material was a direct consequence of shear deformation during drawing. The recrystallization kinetics of the wires upon isothermal annealing at various temperature was influenced by the deformation heterogeneity, and can be accurately described by a modified JMAK-Microhardness model. In this approach, the JMAK model is expressed in terms of microhardness data, from which the parameters of the different restoration kinetics were determined.

Abstract: The effects of strain path reversal under hot working conditions on the microstructure and crystallographic texture in the near-α titanium alloy Timetal-834 have been studied using high resolution electron backscatter diffraction (EBSD). The main objective of the work was to investigate the potential effect strain path may have on breaking up the well known clustering of similarly orientated primary alphas grains in the alloy, which significantly reduces its low cycle dwell fatigue lifetime. Deformation was carried out using forward torsion to an equivalent strain of 0.9 and forward/reverse torsion of two equal steps to produce a total strain of 0.9. The tests were performed at a typical industrial forging condition of 990°C (~50% alpha, ~50% beta) at an equivalent tensile strain rate of 2s-1. Investigation of the microstructure showed the primary alpha grains to align with the direction of torsion for the forward test and return to an equiaxed shape on strain reversal, though a significant numbers of deformation twins are formed and retained after the full strain reversal. Analysis of the texture of the starting material showed the typically clustering of primary alpha grains, which upon forward torsion and forward/reverse torsion did not break down. This indicates that during a typical forging operation the clustering of similarly orientated primary alpha grains inherited from the as-received billet will not be reduced. This suggests that improved in-service performance of this alloy can only be achieved by reducing the clustering upstream in the manufacture of the billet.

Abstract: The influence of strain path during equal-channel angular pressing (ECAP) has been evaluated in pure aluminum by orientation imaging microscopy (OIM) and transmission electron microscopy (TEM). The material was examined after four pressing operations by route BC in a 90° die, or eight pressing operations by route BC in a 135° die. The von Mises equivalent strains were essentially the same for these two ECAP procedures. The microtexture data indicate that the distortion during ECAP corresponds to a simple shear in a direction approximately parallel to diechannel exit and on a plane perpendicular to the flow plane. For both procedures the OIM data reveal prominent meso-scale band-like features. Lattice orientations in each band correspond to a texture orientation but the particular combinations of orientations depend upon ECAP die angle. High-angle boundaries in the structure correspond to interfaces between the bands.

Abstract: Grain boundary engineering has been applied to different materials in order to increase properties particularly sensitive to intergranular phenomena. This work analyses the micromechanisms that allow the control of the amount of special boundaries which respect coincidence site lattice theory. α-brass, a lead alloy, Inconel 625 and Inconel 600 were submitted to different thermomechanical treatments and were analyzed via electron backscatter diffraction in order to characterize their grain boundaries. The occurrence of thin twins in some crystal directions during the deformation step seems to determine the results obtained as well as strain induced boundary migration.

Abstract: The method is described which enables to determine the microtexture that is the orientation distribution within individual grains of a polycrystal. The microtexture is evaluated on the base of X-ray pole distributions measured for separate reflections, referred to as microscopic pole figures (MPF). The procedure for treatment of experimental MPF and the following computation of orientation distribution function is described in detail. Precision of the microtexture evaluation and possible ways of its improvement are discussed. As an example of the method application, orientation distribution within a single grain of aluminum polycrystal deformed by uniaxial compression up to 50% has been examined.

Abstract: This paper studies the microstructure of drawn gold wires to equivalent strain of 10 and to equivalent strain of 8.5 then heat-treated. The texture of gold wire drawn to strain of 10 is mainly composed of <100> and <111> fibers. Tensile strength of the gold wire increases with <111> fiber fraction, while the grain size does not appear to affect the tensile property. With an exception at heat treatment at 600oC, the texture of gold wire drawn the strain of 8.5 is replaced with <100> fiber component by heat treatment process at 400~700oC. Heat treatment at 600oC produces <110> fiber or <112> fiber, depending upon annealing time.