Papers by Keyword: Sintering Method

Abstract: When applied to devices, BaM ferrite materials are required to have magnetic properties such as high saturation magnetization, or microwave properties such as low ferromagnetic resonance linewidth, which require BaM ferrite to be as dense as possible. The density of BaM ferrite can be significantly improved by introducing pre-holding in the sintering process. The density of BaM ferrite can reach 5.06 g/cm³, the sample grain size can reach 100 μm, and the magnetic properties are close to the single crystal state after 1 h of pre-holding. The maximum 4πM_s is 4606 Gs and ΔH is 487 Oe when pre-holding for 1 h, indicating its potential for application in microwave devices.

Abstract: The sintering methods of quartz sand porous ceramics were researched with the low grade quartz sand along the Yangtze River via the vacuum sintering method in this paper, which lay technology foundation for researching new heat insulating materials. The quartz porous ceramics is obtained with the high performance cost, the quartz porous ceramics is sintered at 1050°C via the vacuum conditions, the density of ceramics is 1.267g/cm³, the porosity is 51.6%, the compressive strength is 3.184MPa, the porous ceramics show the homogeneous distribution micro-pore and good shape. The density and the compressive strength of prepared ceramics via the vacuum sintering both are higher than that of prepared ceramics via the atmosphere sintering, however, the porosity is shown the opposite results.

Abstract: Lead-free ceramic powders based on Ba_0.85Ca_0.15Zr_0.1Ti_0.9O₃ (BCZT) were successfully fabricated by the conventional solid-state reaction method. Two kinds of sintering methods: zero-time sintering (ZTS) and conventional sintering (CS) were applied to obtain BCZT ceramics. The microstructure and dielectric properties of BCZT ceramics sintered from the ZTS and the CS method were systematically studied. It was found that the coarse-grained samples with grain sizes ~ 19-21 μm were obtained from the ZTS and the CS method. The CS method with a long time of dwelling was helpful for improving the dielectric properties of lead-free BCZT ceramics. The maximum dielectric constant of 9926 and low dielectric loss of 0.0108 were obtained at CS with 8h.

Abstract: A thin ScSZ electrolyte with a large area was synthesized using the tape-casting method. The conductivity of 0.095 S cm^-1 at 800°C was achieved. The maximum power density of a single cell reached 368 mW cm^-1 at 800°C. To make a large electrolyte battery more suitable, our study improves the casting method of preparing a dense, porous electrolyte substrate that promotes surface roughness of the electrolyte. However, it is difficult to control the thickness of the substrate, meaning that further improvements are needed.

Abstract: Hydroxyapatite (HA) is a biomaterial with excellent biocompatibility. However, the brittleness and low fracture toughness of HA have limited its biomedical applications. As such, HA has been incorporated with zirconia (ZrO2) to enhance its mechanical strength. However, ZrO2 addition decreases the phase stability of HA. HA decomposition is not favored because it decreases the mechanical strength of HA/ZrO2. In this paper, the effect of sintering on HA decomposition is reviewed. Experimental results show that hot isostatic pressing of HA/ZrO2 is one of the most effective methods to suppress HA decomposition, yielding the highest relative density compared with other sintering methods.

Abstract: Hydroxyapatite is a calcium phosphate product that being widely use in medical application due to its excellence biocompatibility. However its application has being limited due to the inferior mechanical properties, many researcher attempted to improve its mechanical properties. HA-ZrO2 composites have great potential because of their advantages from both constituent materials, such as the excellent biocompatibility of HA and the considerable mechanical strength and toughness of ZrO2. The synergy of the two materials provides a new possibility for developing a composite material with better properties than monolithic ZrO2 and HA. In this work, the stages of development, as well as the different sintering and processing methods of HA and ZrO2 such as conventional sintering, solid-state reaction, microwave sintering and hot isostatic pressing were discussed. It can be concluded that hot isostatic pressing processing yield the most satisfying result amount above method, however the use of nano structured material maybe able to provide alternative processing method and yield better result.

Abstract: Abstract: With the industrial development and improvement of mechanical product quality, the demand of part surface quality and accuracy gets more and more high. As some parts of complex shape, can’t be machined by the traditional processing technology, therefore, the magnetic abrasive technique was proposed. The magnetic abrasive particles play an important role in the magnetic abrasive finishing, it use strong magnetic iron particles and abrasive particles mixed together (called magnetic abrasive). The prepared method of magnetic abrasive one of is sintering method, the aim is to change the internal structure of abrasive particles, make the abrasive particles is distributed on the surface of magnetic iron particles, get a kind of magnetic abrasive, which can be magnetized in a magnetic field and improve processing efficiency and surface quality in magnetic abrasive finishing. In this paper, sintering method is used to make iron particles, abrasive particles mixed with some binder, after suppression, drying, sintering, cooling, break up and sieving, analysis surface morphology and composition of the magnetic abrasive particles by scanning electron microscopy, discusses the effect of the abrasive particles size ratio, sintering time, sintering temperature for the finishing performs, the preparation process of the magnetic abrasive has been optimized, work out the standard of preparation of the magnetic abrasive process

Abstract: The magnetic abrasive prepared by sintering method, the aim is to change the internal structure of abrasive particles by sintering method, make the abrasive particles parceled on the surface of magnetic iron particles, and compared with the abrasive particles phase to get a kind of magnetic abrasive particles with high durability, strong magnetic, which can be magnetized in a magnetic field and improve processing efficiency and surface quality in magnetic abrasive machining. Sintering is used to prepare magnetic abrasive in this paper, to make iron particles, abrasive particles mixed with some binder, after suppression, drying, sintering, cooling, crushing and screening. This paper makes analysis for surface morphology and composition of the magnetic abrasive particles by scanning electron microscopy and discusses the effect that the abrasive particles size ratio, sintering time, sintering temperature on the magnetic abrasive, and the preparation of the magnetic abrasive process has been optimized.

Abstract: This paper mainly illustrates the magnetic abrasive finishing by sintering method and research on tests of magnetic abrasive finishing, analyses the effect of the sintering temperature, ratio of magnetic and abrasive particle size, sintering time and sintering characteristics of magnetic particles on magnetic abrasive during the finishing process, so as to achieve a better process and principle for magnetic abrasive finishing.

Abstract: In this paper, ferrosilicon powder was used as the ferromagnetic phase, corundum powder as the abrasive phase, high temperature inorganic binder as the adhesive, and after the ferrosilicon powder was modified, a series of magnetic abrasive was obtained by sintering method. Scanning electron microscope (SEM) and Energy dispersive spectrometer (EDS) were respectively used to characterize the morphology and elemental composition of magnetic abrasive. and through experiments carried out on the magnetic abrasive grinding performance testing and durability analysis. The experimental results showed that the magnetic abrasive prepared had good polishing ability and longer using time, and the surface roughness of the grinding sample can reach 0.12μm and the using time is up to 25 min.