Papers by Keyword: Texture

Abstract: We have reported that development of texture can be controlled by colloidal processing in a strong magnetic field followed by heating even for diamagnetic ceramics such as alumina, titania and so on. We demonstrate in this study that alumina/alumina laminar composites with different crystalline-oriented layer are produced by electrophoretic deposition (EPD) in a strong magnetic field. This composite was fabricated by alternately changing the angle between the directions of the magnetic and electric fields layer by layer during EPD in 12T. The grains in alternate layers are aligned differently.

Abstract: The variations of in plane Charpy toughness anisotropy as a function of the microstructure and texture of an industrial grade of API –X80 pipeline steel was studied. Standard size Charpy samples with a long axis orientated at 0, 22.5, 45, 67.5 and 90° with respect to the rolling direction of the plate were tested at different temperatures varying from -196°C to 20°C. Microstructure and texture of the plates were investigated by means of electron backscattering diffraction (EBSD), XRD and the recently developed 3D EBSD technique. The spatial grain shape orientation distribution was examined on samples which were cut from the middle thickness of an industrial rolled plate by means of 3D EBSD and following grain shape reconstruction and approximation of the grain shape with ellipsoids. It was found that the experimentally observed 3D microstructures could well be correlated to the anisotropy of the measured Charpy impact toughness of the steel for the Charpy samples. The Charpy toughness anisotropy of the plates in the transition region where both ductile and brittle fractures take place can be related to the microstructural anisotropy characterized by the grain shape orientation and the spatial distribution of the 2nd phase.

Abstract: Low alloy transformation induced plasticity (TRIP) steels have a complex microstructure consisting of ferrite, bainite and retained austenite. Their excellent mechanical properties are ascribed to the martensitic transformation of retained austenite during plastic deformation. In the present contribution, the crystallographic texture of fcc and bcc phases in TRIP steels was measured by means of orientation mapping. The austenite texture was close to a typical rolling texture of fcc metals. For bcc phase, the effects of orientation and grain size on the distribution of pattern quality were investigated. The texture of transformation product phase was separated by grain size. The transformation texture showed stronger α fiber including {113}<110> component than the recrystallization texture. It showed a good agreement with a transformation texture predicted by Kurdjmov-Sachs (KS) relationship without any variant selection.

Abstract: Texture and cyclic tensile behavior of Ti-26Nb-0.5Si (denoted as atomic percent) alloys in which the microstructures were varied by quenching, cold rolling and recrystallization heat treatment were investigated in order to understand the relationship between pseudoelastic behavior and texture formation. Three phase mixtures consisting of bcc-structured β phase, orthorhombic structured α" phase and hcp-structured intermediate ω phase were characterized to display the constituent phases. The volume fraction of constituent phases was found to be insensitive to the given materials processing. Two-stage yielding, one at low stress with low strain hardening rate and the other one at high stress with high strain hardening rate, appeared to exhibit a characteristic flow behavior in the present alloys. It is revealed that stress-induced martensite transformation resulting in two-stage yielding was closely associated with pseudoelasticity. On the basis of texture analyses, we have suggested that pseudoelasticity of the present alloys is hindered by the development of {001}<110> rotated cube component.

Abstract: The development of deformation texture and microstructure was examined for four different initial textures. IF steel sheets with a majority of α-, ε-, and γ-fiber and near random texture were prepared and cold rolled. The specimens exhibited characteristic behaviors in rolling texture evolution and deformation-induced misorientation development, according to their initial textures, especially at small strain levels. Due to the orientation dependence of intra-granular misorientation accumulation, the different texture evolutions affected the induced misorientation distribution. A larger fraction of γ-fiber orientations was related to more prominent misorientation development, while the initial texture stability simultaneously affected the misorientation development. The unstable, initial ε-fiber texture showed a stronger tendency of misorientation accumulation than the stable α-fiber during the subsequent cold rolling.

Abstract: The paper deals with the evolution of recrystallization texture during annealing of Equal Channel Angular Extrusion (ECAE) processed copper with different deformation texture that may evolve as a result of different routes of ECAE. The deformation and recrystallization texture components have been separated and corresponding texture analysis has been carried out. An attempt has been made to understand the origin of recrystallization texture.

Abstract: The texture evolution due to grain growth that takes place during annealing was investigated in nanocrystalline Fe-Ni alloys fabricated by using an electroforming method. In the current materials, the as-deposited textures were of fibre-type characterized by strong <100>//ND and weak <111>//ND components, and the occurrence of grain growth during annealing resulted in the strong development of the <111>//ND components with a significant decrease of the <100>//ND components. It was clarified that abnormal grain growth plays an important role on the evolution of the microstructures and textures. The abnormally grown grains were observed using orientation imaging microscopy in the early stages of grain growth, and their morphological features have been discussed.

Abstract: A 2D cellular automaton model developed for the simulation of grain growth in hexagonal metals is presented here. It allows the direct use of experimental measurement as input data. Texture evolution of a titanium alloy and a zirconium alloy are simulated on the basis of simple hypothesis and compared with experimental evolution as well as the results from a 3D Monte Carlo model. Results from both models are discussed with regards to their characteristics.

Abstract: Classical vertex model till now described only the grain growth stage and not the primary recrystallization. In the present work the vertex model is first extended in order to take into account the both stages of recrystallization process. The influence of the stored energy is taken into account and some phenomenological laws describing the evolution of grain boundary energy and mobility with misorientation angle are used. Nucleation is considered to be site-saturated. The experimentally determined stored energy values, crystallographic orientations and boundary misorientation distributions are used in order to characterize the initial microstructure. The model is tested to study the recrystallization of 70% and 90% cold rolled polycrystalline copper during an annealing treatment. In order to explain the texture evolution in both cases, it is necessary to introduce an energy threshold for grain boundary movement, i.e. a minimal value of the stored energy difference between a nucleus and the deformed material necessary to provoke grain boundary motion. The developed model is shown to predict texture evolutions in good agreement with experimental data.