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Preparation and Characterization of Doped Nanometer TiO2
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Preparation and Characterization of Doped Nanometer TiO2

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Abstract:

With Ti(OBu)4 as precursor, and HAC as complexing agent, pure and Fe-doped TiO2 gelatins were prepared by sol-gel method. During the process of gel formation, metal ions were dispersed into the porous TiO2 matrix. Then, powders of pure nano-TiO2 and Fe-doped nano-TiO2 were prepared by drying, grinding and calcining at different temperatures. The grain size and phase structure of pure and Fe-doped TiO2 after calcined at different temperatures, were studied by X-ray diffraction (XRD) and Beckman Coulter Sorption Analysis. The results showed that, the Fe3+-TiO2 had better photocatalytic activity in degradation rate of methyl orange under sunlight. The degradation rate was up to 93% as the system was placed under sunlight for 5 h. The optimum calcination temperature for the best catalytic activity was determined to be 500°C, and the mechanism was discussed.

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Periodical:

Advanced Materials Research (Volumes 26-28)

Pages:

649-652

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.26-28.649

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Online since:

October 2007

Authors:

Lin Yun Song, Yu Cheng Wu, Xiang Fen Lu

Keywords:

Doped, Fe, Sol-Gel (SG), Titania (TiO2)

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© 2007 Trans Tech Publications Ltd. All Rights Reserved

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