Paper Titles
Synthesis of Nanocrystalline 0.94Bi0.5Na0.5TiO3-0.06BaTiO3 Powder by a Citrate Method
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Processing and Properties of Ferroelectric Bi4-x La xTi3O12 Ceramics
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Bi4-xLaxTi3O12 Ferroelectric Thin Films Prepared by RF Magnetron Sputtering
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Preparation and Magnetic Property of Bi2Fe4O9 Nanoparticles by Hydrothermal Method
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Molten Salt Synthesis of CaCu3Ti4O12
p.115
Effects of the Replacement of Ti by Zr on the Dielectric Properties of CaCu3Ti4012 Ceramics
p.118
Effects of CuO on the Preparation, Microstructure and Dielectric Response of CaCu3Ti4O12
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Preparation and Properties of CaCu3Ti4O12 Thick Film by Aerosol Deposition Method
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Molten Salt Synthesis of CaCu3Ti4O12

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Abstract:

CCTO powders were prepared by using molten salt method in the NaCl-KCl system. The effects of temperature and holding time on phase compositions, particle morphology and size have been investigated by X-ray diffraction, scanning electron microscope and laser particle size analyzer. Using CaCO3, CuO and TiO2 as starting materials, CCTO compound could be synthesized at any temperature from 800oC to 1000oC in the NaCl-KCl system. The average particle size increased obviously with the increasing of temperature above 850 oC. Holding time had great effect on grain size and morphology.

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Periodical:

Key Engineering Materials (Volumes 368-372)

Pages:

115-117

DOI:

https://doi.org/10.4028/www.scientific.net/KEM.368-372.115

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Online since:

February 2008

Authors:

Ke Pi Chen, Yong He, Dong Yu Liu, Zong De Liu

Keywords:

CaCu3Ti4O12 (CCTO), Dielectric Constant, Molten Salt Synthesis

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© 2008 Trans Tech Publications Ltd. All Rights Reserved

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References

[1] A. P. Ramirez, M. A. Subramanian, M. Gardel, et al: Solid State Comm. Vol. 115 (2000), p.217.

Google Scholar

[2] M. A. Subramanian, Dong Li, N. Duan, et al: J. Solid State Chem. Vol. 151(2000), p.323.

Google Scholar

[3] D. C. Sinclair, T. A. Adams, F. D. Morrison et al: Appl. Phys. Lett. Vol. 82 (2002), p.2153.

Google Scholar

[4] T. B. Adams, D. C. Sinclair and A. R. West: Adv. Mater. Vol. 14 (2002), p.1321.

Google Scholar

[5] L. Zhang and Z. J. Tang: Phys. Rev. B Vol. 70 (2004), 174306.

Google Scholar

[6] A. R. West, T. B. Adams, F. D. Morrison et al: J. Eur. Ceram. Soc. Vol. 24 (2004), p.1439.

Google Scholar

[7] G. Chiodeli, V. Massarotti, D. Capsoni, et al: Solid State Commun. Vol. 132 (2004), p.241.

Google Scholar

[8] S.Y. Chung, I. -D. Kim and S. J. L. Kang: Nat. Mater. Vol. 3 (2004), p.774.

Google Scholar

[9] X. L. Zhou and P. Y. Du: J. Inorg. Mater. Vol. 20 (2005), p.484.

Google Scholar