Papers by Author: Heinz Günter Brokmeier

Abstract: The materials science diffractometer STRESS-SPEC located at Forschungsneutronen¬quelle Heinz Maier-Leibnitz (FRM-II) in Garching/Germany is a dedicated instrument for residual strain, texture and microstrain analysis. Comparably low gauge volumes of 1x1x1mm³ for gradient investigations in many types of materials can be investigated. A robot system consisting of a robot type Stäubli RX160, a laser tracker and a heavy vibration free basement was installed to overcome limitations in gradient investigations of residual stresses and crystallographic textures in semi-finished and finished products. The robot can carry up to 30kg with precise positioning. Al7020, an Al-alloy for airspace application, was used to perform a first global texture measurement using the robot.

Abstract: Commercial pure magnesium with excellent damping capacity and ZK60 magnesium alloy with high strength were accumulative roll bonded (ARBed) at 300oC up to 3 cycles to fabricate Mg laminate consisting of alternating layers of pure Mg and ZK60. Microstructure, tensile properties and damping capacity of the sheets were analyzed. The research suggests that Mg sheet having both high strength and excellent damping capacity can be developed by accumulative roll bonding of pure Mg and ZK60 Mg alloy.

Abstract: This paper describes microstructure and microtexture development in dissimilar friction welded -TAB-Ti64 joints. The effect of friction welding parameters on microstructure and local properties are examined and discussed. It was found that the intermetallic -TiAl based alloy Ti-47Al-3.5(Mn+Cr+Nb)-0.8(B+Si) (denoted as -TAB) is more sensitive to the applied friction welding parameters used in this study. Furthermore, the bonding between these two alloys was controlled by a diffusion process during a very short process duration. Grain refinement as well microstructure transformation led to local improvement of the friction-welded joints.

Abstract: In order to quantify the plastic anisotropy of the ultrafine grained aluminium alloy AA6016 produced by accumulative roll-bonding (ARB) the Lankford parameter is measured by tensile testing as a function of the number of ARB cycles. The experimental results are compared with those from texture-based Taylor simulations. Increasing differences between experiment and theory at higher number of ARB cycles may be attributed to highly oriented microstructural features.

Abstract: Shot peening is a mechanical surface treatment having a deep impact on the materials which generates beneficial near-surface plastic deformation resulting in changes in peening texture characteristics. The present study aims to investigate the texture gradients in the solution treated (SHT) Ti-2.5Cu after shot peening with Almen intensity of 0.20 mmA. Due to a high transmission and a large beam cross-section of neutrons, texture analysis by neutron diffraction has become the standard method to investigate bulk textures. In contrary, the penetration depth of conventional X-rays is a relatively smaller than that of neutrons. Therefore, it is able to measure texture gradients in some hundred microns from the surface.

Abstract: An extruded AZ80 Mg alloy was utilized to investigate the texture effect on the damping behavior. Results showed that different input textures had great effect on the damping behaviour by strain-depended test, but did not showed strong influence on the temperature-depended behaviour which has been discussed.

Abstract: Equal channel angular pressing (ECAP) was used for grain refinement and texture modification in the initial pressed Mg-Al-Zn alloy to study the possibility to enhance the low-temperature deformability of the material. The effect of different ECAP regimes by routes A, C, and BC on the submicrocrystalline grain formation, texture evolution, and plasticity of the alloy have been investigated. The ECAP of the alloy results in the formation of ultrafine grained structure with a grain size of 0.8-3.5 µm independent of pressing routes and regimes. The ECAP also drastically changes the axial texture by splitting the initial texture characterized by a sharp basal component to several more scattered orientations. The degree of the orientation scattering depends on the ECAP regime and route. It is proposed to estimate the effect of the texture on the yield strength and plasticity of the alloy after ECAP through generalized Schmid factors. The comparable calculated and experimental results are obtained only for yield strength.

Abstract: Crystallographic texture includes much information on a material’s behaviour that depends on the processed material itself, the particular thermomechanical processing it has undergone, and the quality of the process. ECAP processed pure Mg and Mg alloys were characterised by their texture and are discussed in terms of texture symmetry. For all types of deformation, including ECAP, the basal plain orientation has to follow certain general rules. Particularly for larger number of passes the ECAP texture can be explained in terms of standard rolling or extrusion textures.

Abstract: Single pass ECAP of pure Magnesium was performed and stopped after 50 % deformation; textures thereafter at the ingoing, the deformation and the outgoing channel were characterized by neutron radiation and related to the deformation mode. A gradient texture evolution was obtained, which was attributed to the inhomogeneous distribution of the effective stress and strain, and also the inevitable existence of friction.

Abstract: An ultrafine-grained (UFG) Mg-5.0wt%Zn-0.9wt%Y-0.2wt%Zr magnesium alloy with a grain size of about 0.8 µm was produced by subjecting the extruded alloy to equal channel angular pressing (ECAP) for 8 passes at 473 K. Compressive testing was performed on the ECAPed alloy in a temperature range from 423 K to 523 K and under strain rates from 1.67×10-3 to 1.67×10-1 s-1. The ultrafine grains of the ECAPed alloy were stable during compression because of the presence of the dispersion of a fine quasicrystal I-phase and of precipitates in the alloy, which restricted grain growth. The activation energy for the compression at the temperature range from 423 K to 523 K is close to the value for grain boundary diffusion in magnesium, indicating that the compressive deformation is mainly controlled by grain-boundary sliding.