Authors: Brett A. Hull, Joseph J. Sumakeris, Mrinal K. Das, Jim Richmond, John W. Palmour
Abstract: The development of 4H-SiC PiN diodes capable of blocking to greater than 10 kV while
having current ratings of 20 A at 100 A/cm2 is continuing in earnest. VF instability of these diodes
continues to be a roadblock, but progress is being made, and a 20 A/10 kV 4H-SiC PiN diode wafer
with an overall device yield of 40% has been fabricated. The latest device characteristics are
discussed, along with details of approaches in improving the reverse recovery characteristics of
these diodes to satisfy the requirements needed for implementation into high voltage inverter
modules capable of switching at up to 20 kHz.
895
Authors: Qing Chun Jon Zhang, Charlotte Jonas, Bradley Heath, Mrinal K. Das, Sei Hyung Ryu, Anant K. Agarwal, John W. Palmour
Abstract: SiC IGBTs are suitable for high power, high temperature applications. For the first time,
the design and fabrication of 9 kV planar p-IGBTs on 4H-SiC are reported in this paper. A
differential on-resistance of ~ 88 m(cm2
at a gate bias of –20 V is achieved at 25°C, and decreases
to ~24.8 m(cm2
at 200°C. The device exhibits a blocking voltage of 9 kV with a leakage current
density of 0.1 mA/cm2. The hole channel mobility is 6.5 cm2/V-s at room temperature with a
threshold voltage of –6.5 V resulting in enhanced conduction capability. Inductive switching tests
have shown that IGBTs feature fast switching capability at both room and elevated temperatures.
771
Authors: Mrinal K. Das, Sarah K. Haney, Charlotte Jonas, Qing Chun Jon Zhang, Sei Hyung Ryu
Abstract: Optimization of the thermally oxidized 4H-SiC MOS interface has produced p-channel
lateral MOSFETs with hole inversion layer mobility as high as 10 cm2/Vs. This has been
accomplished by identifying the 1200oC Dry, 950oC Wet (un-nitrided) oxidation as ideal for hole
conduction across the MOS inversion layer and by implant activation annealing at 1800oC of the
heavily implanted n-type well. High temperature measurements show that the high mobility and
normally-off operation is maintained throughout the operating temperature range. Oxide leakage
measurements yield a dielectric strength of 8.5 MV/cm with 90% yield, thereby enabling the
manufacture of high performance p-channel devices like the IGBT.
667
Authors: Mrinal K. Das, Brett A. Hull, Sumi Krishnaswami, Fatima Husna, Sarah K. Haney, Aivars J. Lelis, Charles Scozzie, James D. Scofield
Abstract: Two previously reported MOS processes, oxidation in the presence of metallic
impurities and annealing in nitric oxide (NO), have both been optimized for compatibility with
conventional 4H-SiC DMOSFET process technology. Metallic impurities are introduced by
oxidizing in an alumina environment. This Metal Enhanced Oxidation (MEO) yields controlled
oxide thickness (tOX) and robustness against high temperature processing and operation while
maintaining high mobility (69 cm2/Vs) and near ideal NMOS C-V characteristics. Raising the NO
anneal temperature from 1175oC to 1300oC results in a 67% increase in the mobility to 49 cm2/Vs
with a slight stretch-out in the NMOS C-V. Both processes exhibit a small 30% mobility reduction
in MOSFETs fabricated on NA = 1x1018 cm-3 implanted p-wells. The low field mobility in the
MEO MOSFETs is observed to increase dramatically with measurement temperature to 160 cm2/Vs
at 150oC.
967
Authors: Brett A. Hull, Mrinal K. Das, Jim Richmond, Bradley Heath, Joseph J. Sumakeris, Bruce Geil, Charles Scozzie
Abstract: Forward voltage (VF) drift, in which a 4H-SiC PiN diode suffers from an irreversible
increase in VF under forward current flow, continues to inhibit commercialization of 4H-SiC PiN
diodes. We present our latest efforts at fabricating high blocking voltage (6 kV), high current (up to
50 A) 4H-SiC PiN diodes with the best combination of reverse leakage current (IR), forward voltage
at rated current (VF), and VF drift yields. We have achieved greater than 60% total die yield onwafer
for 50 A diodes with a chip size greater than 0.7 cm2. A comparison of the temperature
dependent conduction and switching characteristics between a 50 A/6 kV 4H-SiC PiN diode and a
commercially available 60 A/4.5 kV Si PiN diode is also presented.
1355
Authors: Michael E. Levinshtein, Pavel A. Ivanov, Mykola S. Boltovets, Valentyn A. Krivutsa, John W. Palmour, Mrinal K. Das, Brett A. Hull
Abstract: Steady-state and transient characteristics of packaged 6-kV 4H-SiC junction diodes have
been investigated in the temperature range Т = 300 – 773 К. Analysis of the forward current-voltage
characteristics and reverse current recovery waveforms shows that the lifetimeτ of non-equilibrium
carriers in the base of the diodes steadily increases with temperature across the entire temperature
interval. The rise in τ and decrease in carrier mobilities and diffusion coefficients with increasing
temperature nearly compensate each other as regards their effect on the differential resistance of the
diode, Rd. As a result, Rd is virtually temperature independent. An appreciable modulation of the
base resistance takes place at room temperature even at a relatively small current density j of 20
A/cm2. At T = 800 K and j = 20 A/cm2, a very deep level of the base modulation has been observed.
The bulk reverse current is governed by carrier generation in the space-charge region via a trap with
activation energy of 1.62 eV. The surface leakage current of packaged structures does not exceed
2×10-6 А at T = 773 K and a reverse bias of 300 V.
1339
Authors: Mrinal K. Das, Joseph J. Sumakeris, Brett A. Hull, Jim Richmond
Abstract: The PiN diode is an attractive device to exploit the high power material advantages of
4H-SiC. The combination of high critical field and adequate minority carrier lifetime has enabled
devices that block up to 20 kV and carry 25 A. Furthermore, these devices exhibit fast switching
with less reverse recovery charge than commercially available Si PiN diodes. The path to
commercialization of the 4H-SiC PiN diode technology, however, has been hampered by a
fundamental problem with the forward voltage stability resulting from stacking fault growth
emanating from basal plane screw dislocations (BPD). In this contribution, we highlight the
progress toward producing stable high power devices with sufficient yield to promote commercial
interest. Two independent processes, LBPD1 and LBPD2, have been shown to be effective in
reducing the BPD density and enhancing the forward voltage stability while being compatible with
conventional power device fabrication. Applying the LBPD1 and LBPD2 processes to 10 kV (20 A
and 50 A) 4H-SiC PiN diode technology has resulted in a dramatic improvement in the total device
yield (forward, reverse, and forward drift yields) from 0% to >20%. The LBPD1 process appears to
be more robust in terms of long term forward voltage stability.
1329
Authors: Sei Hyung Ryu, Sumi Krishnaswami, Brett A. Hull, Bradley Heath, Mrinal K. Das, Jim Richmond, Anant K. Agarwal, John W. Palmour, James D. Scofield
Abstract: 8 mΩ-cm2, 1.8 kV power DMOSFETs in 4H-SiC are presented in this paper. A 0.5 μm
long MOS gate length was used to minimize the MOS channel resistance. The DMOSFETs were
able to block 1.8 kV with the gate shorted to the source. At room temperature, a specific onresistance
of 8 mΩ-cm2 was measured with a gate bias of 15 V. At 150 oC, the specific onresistance
increased to 9.6 mΩ-cm2. The increase in drift layer resistance due to a decrease in bulk
electron mobility was partly cancelled out by the negative shift in MOS threshold voltage at
elevated temperatures. The device demonstrated extremely fast, low loss switching characteristics.
A significant improvement in converter efficiency was observed when the 4H-SiC DMOSFET was
used instead of an 800 V silicon superjunction MOSFET in a simple boost converter configuration.
1261
Authors: Bernard F. Phlips, Karl D. Hobart, Francis J. Kub, Robert E. Stahlbush, Mrinal K. Das, Gianluigi De Geronimo, Paul O' Connor
Abstract: We have tested the radiation detection performance of Silicon Carbide (SiC) PIN diodes
originally developed as high power diodes. These devices consist of 100 micron thick SiC grown
epitaxially on SiC substrates. The size and thickness of the devices make them appropriate for a
number of radiation detection applications. We tested 0.25 cm2 and 0.5 cm2 devices and obtained
X-ray spectra under illumination with an Am-241 radioactive source. The spectra showed an energy
resolution that was consistent with the resolution expected for the large capacitance of the device.
Smaller devices with a diameter of 1 mm were also tested and produced spectra with a room
temperature energy resolution of ~550 eV, which is consistent with the electronics limit for the
capacitance of the small device. We measured the absolute charge generated by X-rays per KeV in
SiC by comparing the charge generation with similar silicon devices and determined the energy
required per electron hole pair in SiC to be 8.4 eV. We also performed radiation damage tests on
these devices and found no significant loss in charge collection up to a photon dose of 100 MRad.
Applications for these devices can be found in the fields of particle physics, nuclear physics,
nuclear medicine, X-ray fluorescence, X-ray astronomy and X-ray navigation.
1465
Authors: Joseph J. Sumakeris, Peder Bergman, Mrinal K. Das, Christer Hallin, Brett A. Hull, Erik Janzén, H. Lendenmann, Michael J. O'Loughlin, Michael J. Paisley, Seoyong Ha, Marek Skowronski, John W. Palmour, Calvin H. Carter Jr.
Abstract: Forward voltage instability, or Vf drift, has confounded high voltage SiC device makers
for the last several years. The SiC community has recognized that the root cause of Vf drift in
bipolar SiC devices is the expansion of basal plane dislocations (BPDs) into Shockley Stacking
Faults (SFs) within device regions that experience conductivity modulation. In this presentation,
we detail relatively simple procedures that reduce the density of Vf drift inducing BPDs in epilayers
to <10 cm-2 and permit the fabrication of bipolar SiC devices with very good Vf stability. The first
low BPD technique employs a selective etch of the substrate prior to epilayer growth to create a
near on-axis surface where BPDs intersect the substrate surface. The second low BPD technique
employs lithographic and dry etch patterning of the substrate prior to epilayer growth. Both
processes impede the propagation of BPDs into epilayers by preferentially converting BPDs into
threading edge dislocations (TEDs) during the initial stages of epilayer growth. With these
techniques, we routinely achieve Vf stability yields of up to 90% in devices with active areas from
0.006 to 1 cm2, implying that the utility of the processes is not limited by device size.
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