Authors: Xing Hai Shao, Jing Pei Xie, Wen Yan Wang, Yan Li, Pin Gan Zhou, Hui Wu Yu
Abstract: The effects and the mechanisms of namo TiN on the high chromium cast iron are studied, the material has been prepared through infiltration casting and addition of high carbon ferrochrome powder and nano TiN powder. The alloy is formed on the surfaced of guide plate, and the wear resistance of alloy have been studied by means of SEM, XRD micro-analysis and wear-resistant performance. The grain size and the type of carbide in the organization are affected by nano TiN, and the wear resistance of carbon chromium alloy layer is affected by the type of carbide; when the addition of nano TiN is 1% (wt), the grain size is apparently refined, overeutectic primary M7C3 in the hypereutectic is precipitated uniformly in considerable amounts, therefore the wear resistance of alloy can be improved effectively.
2410
Authors: Hui Wu Yu, Wen Yan Wang, Jing Pei Xie, Pin Gan Zhou, Yan Li, Jia Xi Wang, Xing Hai Shao
Abstract: The ZGMn13Cr2 reinforced by the nano-SiC master alloy is investigated in this paper. The nano-SiC master alloy which comprise nano-SiC powders and other metal powders are prepared, then the nano-SiC master alloy is added into the ZGMn13Cr2 samples under industrial conditions. The morphology and mechanical properties of the samples are studied. The results show that: When the nano-SiC Master Alloy is added into the sample, the microstructure of ZGMn13Cr2 improve significantly and the absorbed energy of the samples increased obviously.
404
Authors: Yan Li, Jing Pei Xie, Hui Wu Yu, Wen Yan Wang, Xin Hai Shao, Luo Li Li, Ai Qin Wang, Ji Wen Li
Abstract: Mn18Cr2 steel is one of austenitic deformation strengthening steel. The existing form of TiN and its influence on the austenitic structure in the steel by adding small amounts of TiN nanoparticles are discussed in this study, which may provide some advices to explore new way to strengthen high manganese steel. The microstructures of Mn18Cr2 steel added small amounts of TiN nanoparticles are observed by Transmission Electron Microscopy (TEM). The results show that TiN nanoparticles exist in austenite and there have a very good match interface between the two phases, the crystal face relationship are {220}γ//{220}N, {422}γ//{422}N, (111)γ //(200)N , orientation relationship are <110>γ// <110>N, <211>γ//<211>N, [112]γ // [011]N, moreover, the relationship of (111)γ and (200)N is not only parallel but also coherent. Meanwhile, there are many high density dislocations, a small amount of stacking faults, twins and ε-martensite in the austenite due to the role of TiN nanoparticles.
897
Authors: Ai Qin Wang, Jing Pei Xie, Wen Yan Wang, Ji Wen Li, Luo Li Li
Abstract: A rapid-solidified hypereutectic Al-21Si-0.8Mg-1.5Cu-0.5Mn alloys strips has been prepared by single roller melt-spinning. The effects of solution technology on the microstructures and properties of the strips have been investigated by SEM, TEM. The results showed that the nucleation and growth of primary silicon are suppressed and α-Al is nucleated which prior to eutectic. The Cu, Mg and Mn are all supersaturated solution in α-Al. The major part of Si solution in α-Al, and the rest are precipitated by the micro-nanocrystals eutectic silicon. The metastable microstructures of micro-nanocrystals hypoeutectic are formed. And in the solution process, Si are precipitated from the matrix and gradually aggregate up to form small particles distributing in the matrix with the heating time. At 480°C for 100 minutes followed by quenching in water and a natural aging for 96h, the finer and more roundness of silicon particle and the maximum Vickers hardness are formed.
243
Authors: Ji Wen Li, Ai Qin Wang, Jing Pei Xie, Wen Yan Wang, Luo Li Li
Abstract: Rapidly solidified hypereutectic Al-21Si was prepared by the single roller melt-spinning technique. The microstructure morphology characteristics and phase structures of the alloy were characterized using SEM, TEM and XRD technique. The results showed that the grains were refined and the micro-nano composite structures were formed under rapid solidification. The microstructure of the Al-21Si alloy was composed of micro-nanostructured α-Al phase and feather-needle-like eutectic α-Al+β-Si phase. The α-Al phase was the leading phase in the eutectic α+Si phase. The nucleation and growth of primary silicon are suppressed and primary silicon could not be precipitated. The hypereutectic Al-21Si alloy showed the hypoeutectic solidification microstructure. Wear resistance was improved obviously when the rapidly solidified and was five times higher than that of the traditional casting alloys.
986
Authors: Wen Yan Wang, J. Xu, Jing Pei Xie, H. Yan, A.H. Wang
Abstract: Nickel-based nano self-lubricating coatings were deposited on medium carbon steel by laser. The microstructure and tribological properties of the typical coating containing 10wt % nano-hBN powders were investigated using SEM incorporating EDS, and high temperature tribo-tester, respectively. It was found that the cladding layer and substrate was good metallurgical bonding. Dry sliding frictional tests suggested that the composite coating containing about 10wt % hBN powders has lower friction coefficient than that of pure Ni60 cladding at room temperature with a load of 40N and a speed of 2m/s, as well as 400°C with a load of 20N and a speed of 2m/s. The wear resistance of Ni60-hBN coating is about 10 times than that of Ni60 coating. The SEM analysis of the abrasion morphology found that wear mechanism of self-solid lubrication coating was adhesive wear, and wear mechanism of the cladding layer of non-lubricant was adhesive wear with abrasive wear.
421
Authors: Jing Xu, Wen Yan Wang, Jing Pei Xie, Ji Wen Li, Ai Qin Wang
Abstract: The wear resistance, corrosion resistance, high temperature resistance layers were prepared on the surface of ductile iron via laser alloying process, using the mixed ponder of sub-micron carbides power as starting materials. The microstructures of the different laser alloying layers were characterized by XRD, SEM, EDS, TEM. The microhardness and wear resisitance of the laser alloying layers were examined. The results reveal that the flat alloyed coating combines metallurgically with the substrate. the laser area was composed by alloyed zone ,heat-affected zone and matrix zone. The alloyed zone was composed mainly by ledeburite and carbide, while martensite and retained austenite were contained in the heat affected zone, there is no significant change in the Matrix zone. Under conditions that the laser power, spot diameter remain unchanged, with in 400 ~ 1000 mm/min scanning speed, the hardness of alloyed coating increases with increasing scanning speed. The weightlessness of the alloyed samples under the dry sliding friction is one-sixteenth of ductile iron. The wear resisitance of the alloyed coating has improved significantly.
413
Authors: Jing Pei Xie, Shu Qing Yan, Ai Qin Wang, Wen Yan Wang, Gi Wen Li, Xiao Li Li
Abstract: The microstructures characteristics of interface and wear resistance Of ZnAl27 composite reinforced by SiC particles have been studied by means of SEM and HRTEM. The results shown that SiC particles could be distributed in ZnAl27 alloy uniformly, and the excellent combined interface between SiC particles and ZA27 matrix is formed. CuZn4 could nucleate on SiC particles and grow up at higher speed along SiC particles than at the vertical direction. The wear resistance of the ZnAl27 alloy could be increased remarkably due to the addition of SiC particles. When the SiC particles are added to 30%, the wear resistance was raised by 126.5 times
1871
Authors: Shu Qing Yan, Jing Pei Xie, Wen Yan Wang, Ji Wen Li
Abstract: In this study, some low-titanium aluminum alloys produced by electrolysis were prepared and the effect of various titanium contents on microstructure and tensile property of Zn-Al alloy was investigated. The test results showed that addition of titanium by electrolysis is an effective way to refine the grain size of Zn-Al alloy. As the titanium content is 0.04 wt%, the grain size becomes to be a minimum value and the tensile property of the alloy reaches to the maximum. Electrolysis showed that titanium atoms are to be some inherent particles in low-titanium aluminum alloy. These titanium atoms enter into the aluminum melt liquid and spread to the whole melt rapidly under stirring action of electromagnetic field of the electric current. The heterogeneous phase nuclei are high melting TiC and TiAl3 particles formed from in-situ precipitating trace C and Ti during cooling process. These in-situ precipitating heterogeneous nucleation sites with small dimension, high dispersity, cleaning interface and fine soakage with melt, have better capacity of heterogeneous nucleation than of exotic particles. It may inhibit grain growth faster and more effective in pinning dislocations, grain boundaries or sub-boundaries.
1415
Authors: Ai Qin Wang, Ji Wen Li, Jing Pei Xie, Wen Yan Wang
Abstract: In the present work, rapidly solidified hypereutectic Al-Si-Cu-Mg alloys strips was prepared by single roller melt-spinning method. The microstructures, phase and morphology characteristics of the resultant strips were characterized by means of SEM, TEM and XRD technique. The results show that the grains are refined after rapid solidification processing, and the micro-nanocrystals are formed. Compared with equilibrium solidification, the microstructures are changed obviously. The nucleation and growth of primary silicon are suppressed and primary silicon can not deposited, meanwhile, α-Al phase is nucleated which prior to eutectic. Therefore, the microstructures become into the metastable state. The microstructures of the strips are composed of primary micro-nanostructure α phase and feather-needles-like (α+Si) eutectic which set in the α phase. The mechanism of the formation for microstructures of melt-spinning Al–Si alloy have also been discussed.
139