Papers by Keyword: Crystallographic Texture

Abstract: In Nd9.5Fe84B6.5 melt-spun ribbon, the quenching temperature is found to be effective for the texture development of Nd2Fe14B nanocrystals. For a relatively low quenching temperature of 1250°C a (00l) texture of Nd2Fe14B crystals was found on the free-side surface of the ribbons. At a higher quenching temperature of 1350°C, the microstructure of the free-side surface of the ribbons switches into (320) and (517) texture. It is believed that the transformation of the melt at higher temperature triggers the switch of the texture.

Abstract: The materials science diffractometer STRESS-SPEC located at Forschungsneutronen¬quelle Heinz Maier-Leibnitz (FRM-II) in Garching/Germany is a dedicated instrument for residual strain, texture and microstrain analysis. Comparably low gauge volumes of 1x1x1mm³ for gradient investigations in many types of materials can be investigated. A robot system consisting of a robot type Stäubli RX160, a laser tracker and a heavy vibration free basement was installed to overcome limitations in gradient investigations of residual stresses and crystallographic textures in semi-finished and finished products. The robot can carry up to 30kg with precise positioning. Al7020, an Al-alloy for airspace application, was used to perform a first global texture measurement using the robot.

Abstract: The genetic algorithm method was used in the present work as an alternative to classical calculation methods. It can be used in the situations where we search an optimal solution and a problem has many variable parameters. In this work the genetic algorithm method was applied in order to decompose the texture function into ideal components and also to optimize elastic constants by an appropriate choice of texture function. These example applications of genetic algorithm method show its potential in the field of material engineering.

Abstract: In this contribution, the prediction of the self-consistent homogenization method with regard to the effective material response of cubic crystal aggregates is analyzed and compared to results from full field simulations. The influence of the crystalline orientation distribution but also the effect of the grain shape on the macroscopic elastic response of sheet metals is especially emphasized.

Abstract: ray diffraction method is used to determine the stress field in polycrystalline materials. The measurement of peak shifts enables the determination of the macrostresses and the plastic incompatibility stresses (intergranular stresses). In the interpretation of the experimental results self-consistent model of elatoplastic deformation is used. In the present work, the plastic incompatibility stresses and the elastic energy stored in cold rolled brass and ferritic steel were determinate. The results are discussed and presented in Euler space.

Abstract: Large-diameter steel pipes are produced by induction seam-welding followed by induction-assisted heat treatment. The microstructure and distribution of crystal orientations have been studied and related to the mechanical properties of the welded regions. The welding and heat-treatment process leads to a microstructure, a simple observation of which can not explain the observed variations in toughness in the vicinity of the welding joint, because the crystallographic grain size, which represents the scale of similarly oriented adjacent grains, is much coarser than the ordinary grain size. Furthermore, heating the affected zone into the austenite phase field followed by cooling does not completely eliminate the coarse regions of similarly oriented grains. The consequences of this on mechanical properties are discussed.

Abstract: In this article we present the results of the experimental research and those of the processes developing the crystallographic texture of computer modeling in CP Ti in the process of 1-4 equal channel angular pressing (ECAP) passes along the route ВС. The goal of the research was to determine the active deformation mechanisms, depending on the strain degree, accumulated in the ECAP process. The research was carried out by the method of X-ray analysis and by computer modeling. Computer modeling was carried out on the example of visco-plastic self-consistent model. Thereby, the basal, the prismatic and the pyramidal (of the 1st and of the 2nd order) slip systems were considered as possible active slip systems. Besides, the possibility of activating the tensile and the compressive twinning systems were taken into consideration. As the result of the carried out experimental research, the objective laws of forming preferred orientations were determined. For the first time, with the help of computer modeling, made up to the 4th ECAP pass, it was shown that the crystallographic texture development processes in CP Ti in ECAP, realized at temperature of 723 K, can be explained by activation of the basal, prismatic and pyramidal (of the 1st order) slip systems and compressive twinning systems. Therefore, the increase of the ECAP passes can lead to amplification of contribution of the basal and prismatic slip systems, as well as the insignificant weakening of the contribution of pyramidal slip systems (of the 1st order). Moreover, the compressive twinning can become obvious only in the 1st ECAP pass.

Abstract: Crystallographic texture includes much information on a material’s behaviour that depends on the processed material itself, the particular thermomechanical processing it has undergone, and the quality of the process. ECAP processed pure Mg and Mg alloys were characterised by their texture and are discussed in terms of texture symmetry. For all types of deformation, including ECAP, the basal plain orientation has to follow certain general rules. Particularly for larger number of passes the ECAP texture can be explained in terms of standard rolling or extrusion textures.

Abstract: Relatively high mechanical strength and simultaneously good plasticity of a crystalline material are determined by the state of its internal structure, preferably nano- or ultra-fine grained one. To achieve the above combination of properties, various manners of plastic deformation and heat treatment are applied in practice. One of the most effective processes in this field is severely plastic deformation, e.g. by the method of equal angular channel pressing (ECAP). During the ECAP, favourable effects of grain fragmentation and the formation of specific orientation relations can be attenuated by the process of structure recovery, especially, when the real temperature of angular extrusion is elevated for physical or technological reasons. An attempt to modify the ECAP technology was considered, to avoid the unfavourable temperature effects and to increase at the same time the efficiency of manufacturing the ultra-fine structure of material. Extrusion of dual-material (AZ31 + Al) ingot was performed at room temperature. As it seems, the well known difficulties with plastic deformation of materials with hexagonal lattice symmetry, like AZ31 alloy, have been decreased. Both experimental and methodological aspects of the angular extrusion of the dual-material ingot and chosen microstructure characteristics (texture, stress, morphology) are presented. On the basis of the suggested modification, the text discusses an explanation of physical origins of the microstructure evolution in the investigated material revealed by experiments.

Abstract: By associating texture determinations and strains measurements by neutron diffraction, the elastoplastic behaviours of families of crystallites with the same crystallographic orientations were characterized in situ in a brass and a bronze alloys under uniaxial loading. The polycrystalline orientation analysis method proposed here allows an intermediate approach between a “local” (intragranular) and a “global” characterization, within the bulk of massive samples.