Free Volume Study of Severely Plastic Deformed Pure Fe

Article Preview

Abstract:

There is a growing interest for investigation of free-volume type defects in SPD-processed ultrafine-grained materials. In the present work, excess free volume in pure Fe prepared by shaped rolling is studied by high-resolution differential dilatometer as well as Archimedes method. The results show the formation of excess volume with increasing deformation strain. The volume fraction of free volume detected by dilatometer is below the evaluation of Archimedes method maybe because of the existence of void in the deformed metal. Microstructural study by field emission type scanning electron microscope confirms the presence of voids.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

110-114

Citation:

Online since:

November 2013

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] H.E. Schaefer, R. Wurschum, P. Hof, W. Straub, T. Gessmann, Size distribution of structural free volumes in nanocrystalline metals, Mater. Sci. Forum 175-178 (1995) 505-508.

DOI: 10.4028/www.scientific.net/msf.175-178.505

Google Scholar

[2] B. Oberdorfer, B. Lorenzoni, K. Unger, W. Sprengel, M. Zehetbauer, R. Pippanc, R. Wurschum, Absolute concentration of free volume-type defects in ultrafine-grained Fe prepared by high-pressure torsion, Scr. Mater. 63 (2010) 452-455.

DOI: 10.1016/j.scriptamat.2010.05.007

Google Scholar

[3] J. Ribbe, D. Baither, G. Schmitz, S.V. Divinski, Ultrafast diffusion and internal porosity in ultrafine-grained copper–lead alloy prepared by equal channel angular pressing, Scr. Mater. 61 (2009) 129–132.

DOI: 10.1016/j.scriptamat.2009.03.029

Google Scholar

[4] I. Sabirov, M. Yu. Murashkin, R.Z. Valiev, Nanostructured aluminium alloys produced by severe plastic deformation: New horizons in development, Mater. Sci. Eng. A 560 (2013) 1–24.

DOI: 10.1016/j.msea.2012.09.020

Google Scholar

[5] M. Krystian, D. Setman, B. Mingler, G. Krexner, M.J. Zehetbauer, Formation of superabundant vacancies in nano-Pd–H generated by high-pressure torsion, Scr. Mater. 62 (2010) 49–52.

DOI: 10.1016/j.scriptamat.2009.09.025

Google Scholar

[6] T.D. Shen, J. Zhang, Y. Zhao, What is the theoretical density of a nanocrystalline material?, Acta Mater. 56 (2008) 3663–3671.

DOI: 10.1016/j.actamat.2008.04.003

Google Scholar

[7] R. Wurschum, B. Oberdorfer, E-M Steyskal, W. Sprengel, W. Puff, Ph. Pikart, Ch. Hugenschmidt, R. Pippan, Free volumes in bulk nanocrystalline metals studied by the complementary techniques of positron annihilation and dilatometry, Physica B 407 (2012).

DOI: 10.1016/j.physb.2012.01.090

Google Scholar

[8] G.K. Williamson, W.H. Hall, X-ray line broadeningfrom filed Al and W, Acta Metall. 1 (1953) 22–31.

Google Scholar

[9] A. Mirsepasi, M. Nili-Ahmadabadi, M. Habibi-Parsa, H. Ghasemi-Nanesa, A. F. Dizaji, Microstructure and mechanical behavior of martensitic steel severely deformed by the novel technique of repetitive corrugation and straightening by rolling, Mater. Sci. Eng. A 551 (2012).

DOI: 10.1016/j.msea.2012.04.073

Google Scholar

[10] J. Inoue, Y. Fujii, T. Koseki, Void formation in nanocrystalline Cu film during uniaxial relaxation test, Acta Mater. 56 (2008) 4921–4931.

DOI: 10.1016/j.actamat.2008.06.008

Google Scholar

[11] S.V. Divinski, K.A. Padmanabhana, G. Wilde, Microstructure evolution during severe plastic deformation, Philos. Mag. (2011) 1–20.

Google Scholar