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Sintering Behavior and Mechanism of Pure BaTiO3 Ceramic Prepared by High-Gravity Reactive Precipitation
Abstract:
Sintering behavior and mechanism of barium titanate powders prepared by high-gravity reactive precipitation (HGRP) process has been investigated by a dilatometer. The mean particle size of barium titanate powders prepared by HGRP was about 80 nm. Pure BaTiO3 pellets were sintered at a constant heating rate of 2.0 K/min and the temperature of shrinkage-onset for pellet was 1060°C. The maximal shrinkage was 165um and the maximum of shrinkage rate was 8.0 x 10-3 / min at 1170°C. The sintering mechanism for the initial stages of sintering was determined by isothermal dilatometric measurements and was found to be viscous flow.
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27-30
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February 2006
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© 2006 Trans Tech Publications Ltd. All Rights Reserved
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