Effect of Heat Treatment on Microstructure Homogeneity of Zn-3Mg Alloy

Article Preview

Abstract:

The Zn based alloy has a high potential to be the next generation of biodegradable implant material. Development of this biomaterial involves casting process which often associated with various defects. In this study, Zn-3Mg alloy was prepared using conventional casting method and followed by homogenization treatment (370°C for 10hr) with the aim to improve the microstructure uniformity. Microscopic images show that as-cast Zn-3Mg alloy consists of segregated Zn-rich structure of star-like dendritic shape and eutectic mixture of Mg2Zn11 phase. It is observed that after the heat treatment process thissegregation has been dispersed well and results in a more uniform microstructure of Zn-3Mg alloy with low fraction of casting defects.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

777-782

Citation:

Online since:

January 2014

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] M Geethaa, AK Singh, R Asokamani, AK Gogia, Ti based biomaterials, the ultimate choice for orthopaedic implants – A review, Progress in Materials Science. 54 (2009), pp.397-425.

DOI: 10.1016/j.pmatsci.2008.06.004

Google Scholar

[2] FM Nor, D Kurniawan, YK Seo, JK Park, HY Lee, JY Lim, Polycaprolactone–starch blends with corn-based coupling agent: physical properties and in vitro analysis, Proceedings of the Institution of Mechanical Engineers, Part H: Journal of Engineering in Medicine. 226 (2012).

DOI: 10.1177/0954411912452988

Google Scholar

[3] D Kurniawan, FM Nor, HY Lee, JY Lim, Elastic properties of polycaprolactone at small strains are significantly affected by strain rate and temperature, Proceedings of the Institution of Mechanical Engineers, Part H: Journal of Engineering in Medicine. 225 (2011).

DOI: 10.1177/0954411911413059

Google Scholar

[4] PK Bowen, J Drelich, J Goldman, Zinc Exhibits Ideal Physiological Corrosion Behavior for Bioabsorbable Stents, Adv. Materials. 10 (2013) pp.20-26.

DOI: 10.1002/adma.201300226

Google Scholar

[5] ZG Huan, MA Leeflang, J Zhou, LE Fratila-Apachitei, J Duszczyk, In vitro degradation behavior and cytocompatibility of Mg-Zn-Zr alloys, J Mater Sci Mater Med. 21 (2010) pp.2623-2635.

DOI: 10.1007/s10856-010-4111-8

Google Scholar

[6] X Gu, Y Zheng, Y Cheng, S Zhong, T Xi, In vitro corrosion and biocompatibility of binary magnesium alloys, Biomaterials. 30 (2009) pp.484-98.

DOI: 10.1016/j.biomaterials.2008.10.021

Google Scholar

[7] E Zhang, WW He, H Du, K Yang, Microstructure, mechanical and corrosion properties of Mg-Zn-Y alloys with low Zn content, Materials Science and Engineering. 488 (2008) p.102–111.

DOI: 10.1016/j.msea.2007.10.056

Google Scholar

[8] E Zhang, L Yang, J Xu, H Chen, Microstructure, mechanical properties and biocorrosion properties of Mg–Si(–Ca, Zn) alloy for biomedical application, Acta Biomater 6 (2010) pp.1756-1762.

DOI: 10.1016/j.actbio.2009.11.024

Google Scholar

[9] S Zhang, X Zhang, C Zhao, J Li, Y Song, C Xie, H Tao, Y Zhang, Y He, Y Jiang, Y Bian, Research of Mg–Zn alloy as a degradable biomaterial, Acta Biomater. 6 (2010) pp.626-640.

DOI: 10.1016/j.actbio.2009.06.028

Google Scholar

[10] KM Hambidge, NF Krebs, Zinc deficiency: a special challenge, J. Nutrition. 137 (2007) pp.1101-1105.

Google Scholar

[11] XN Gu, N Li, YF Zheng, L Ruan, In vitro degradation performance and biological response of a Mg-Zn-Zr alloy, Materials Science and Engineering B. 176 (2011) pp.1778-1784.

DOI: 10.1016/j.mseb.2011.05.032

Google Scholar

[12] D Vojtech, J Kubasek, J Serak, P Novek, Mechanical and corrosion properties of newly developed biodegradable Zn-based alloys for bone fixation, Acta Biomater. 7 (2011) pp.3515-3522.

DOI: 10.1016/j.actbio.2011.05.008

Google Scholar

[13] MB Karamış, İ Halıcı, The effects of homogenization and recrystallization heat treatments on low-grade cold deformation properties of AA 6063 aluminum alloy, Materials Letters. 61 (2007) pp.944-948.

DOI: 10.1016/j.matlet.2006.06.016

Google Scholar

[14] BK Prasad, Influence of heat treatment parameters on the lubricated sliding wear behavior of a zinc-based alloy, Wear. 257 (2004) pp.1137-1144.

DOI: 10.1016/j.wear.2004.07.006

Google Scholar

[15] NC Hosking, MA Stron, PH Shipway, CD Rudd, Corrosion resistance of zinc-magnesium coated steel, Corr. Sci. 49 (2007) pp.3669-3695.

DOI: 10.1016/j.corsci.2007.03.032

Google Scholar

[16] B Biljana, B Jelena, Z Acimovic-pavlovic, R Marko, B Ilija, The effect of T4 heat treatment on the microstructure and corrosion behaviour of Zn27Al1. 5Cu0. 02Mg alloy, Corrosion Science. 53 (2011) pp.409-417.

DOI: 10.1016/j.corsci.2010.09.051

Google Scholar

[17] Y Xinqi, L Shengxin, L Weimin, H Junlan, Z Liangying, C Yong, The effect of homogenization treament on icrostructure and properties of ZnAl15 solder, Materials and Design 45 (2013) pp.440-445.

Google Scholar

[18] K Kotah, K Kojima, H Ishimoto, T Yashiki, Development of corrosion preventive Zn-Mg thermal sprayed steel plate for oil storage tanks, Journal of High Pressure Institute of Japan. 42 (2004) pp.207-221.

Google Scholar

[19] X Wang, H Lu, X Li, L Li, Y Zheng, Effect of cooling rate and composition on microstrcutures and properties of Zn-Mg alloys, Trans. Nonferrous Met. Soc. China. 17 (2007) p. s122-s125.

Google Scholar