The Synthesis of High Yield Diglycerin Borate

Qi Wang; Guo Zheng; Jian Jie Ai; Xue Jing Wei

doi:10.4028/www.scientific.net/AMM.55-57.312

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HomeApplied Mechanics and MaterialsApplied Mechanics and Materials Vols. 55-57The Synthesis of High Yield Diglycerin Borate

The Synthesis of High Yield Diglycerin Borate

Abstract:

High yield diglycerin borate(DGB) have been synthesized by the raw materials glycerol and boric acid in this paper. The structure of the products was characterized by FTIR and ¹¹B NMR. The yield of the products was discussed by reaction conditions that were material ratio, reaction temperature, reaction pressure etc. and then the optimum process conditions of preparing DGB was decided. In this condition, high yield DGB can be prepared which could reach more than 96%.

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Periodical:

Applied Mechanics and Materials (Volumes 55-57)

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312-316

DOI:

https://doi.org/10.4028/www.scientific.net/AMM.55-57.312

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Online since:

May 2011

Authors:

Qi Wang, Guo Zheng, Jian Jie Ai, Xue Jing Wei

Keywords:

¹¹B NMR Spectrum, Boric Acid, Diglycerin Borate, Glycerol

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