Solvothermal Synthesis of Size-Controlled Lead Zirconate Titanate Particles

Fan Zhang; Zhan Jie Wang

doi:10.4028/www.scientific.net/AMM.675-677.27

Paper Titles

CO₂ Absorption/Release Properties of Lithium Silicate (Li₂SiO₃) Powders Prepared by the Sol-Gel Process
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Properties of Resistance Spot Welded Joint between Mild Steel and Aluminum Alloy with an Interlayer of AlCu28
p.15

Resistance Spot Welding between Copper Coated Steel and Aluminum Alloy
p.19

Resistance Spot Welding between Mild Steel and Stainless Steel
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Solvothermal Synthesis of Size-Controlled Lead Zirconate Titanate Particles
p.27

Surface Wettability of the Contaminative Silicone Rubber
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The Formation of Coesite under Minimum Static Pressure
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Measurement System Research on Micro-Arc Oxidation Load Feature
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Mechanical Behavior of a Dissimilar Metal Weld Used for Nuclear Power Plants
p.47

HomeApplied Mechanics and MaterialsApplied Mechanics and Materials Vols. 675-677Solvothermal Synthesis of Size-Controlled Lead...

Solvothermal Synthesis of Size-Controlled Lead Zirconate Titanate Particles

Abstract:

Nanocrystalline lead zirconate titanate (PZT) powders have been synthesized by solvothermal method, in which a mixed solvent of ethanol and water was used as reactive medium and Pb (NO₃)₂, ZrOCl₂·8H₂O, C₁₆H₃₆O₄Ti, KOH and NH₃·H₂O were used as raw materials. It was found that PZT particle sizes decreased from 2 μm to 100 nm with the ratio of V_ethanol/V_water increasing from 1/2 to 2/1 under a KOH concentration of 4 mol/L at 200 °C for 4 h. It indicated that the V_ethanol/V_water of mixed solvent played an important role in controlling the morphology and size of PZT crystals, as well as reaction temperature.