Study on the Determination of Cypermethrin Residues in Vegetable

Ru Ling Zhang

doi:10.4028/www.scientific.net/AMM.686.73

Paper Titles

Evaluation of Asphalt-Aggregate Adhesion Using Surface Free Energy Theory
p.51

Study on Preparation of Ceramic Material and its Properties
p.57

Research on Polymer Materials in Bio Medical and its Application
p.61

Oxidative Desulfurization Performance Optimization of Tert-Amyl Hydroperoxide
p.66

Study on the Determination of Cypermethrin Residues in Vegetable
p.73

The Description of Precision Forging Technology in Closed Die of Mg Alloy AZ31 Using Computer Simulation
p.78

Texture Classification of 3D Surface Textures via Directional Quincunx Lifting
p.82

Study on Fuzzy Immune PID Controller for Main Steam Pressure Control System in Marine Steam Power Plant
p.89

An Application of Fuzzy Logic Control Algorithm in Hydro Mechanical Deep Drawing Process
p.95

HomeApplied Mechanics and MaterialsApplied Mechanics and Materials Vol. 686Study on the Determination of Cypermethrin...

Study on the Determination of Cypermethrin Residues in Vegetable

Abstract:

The paper establish an analysis method for determination Cypermethrin pesticide residue in vegetable. Using acetonitrile to extract cypermethrin in vegetable, and purified by Agilent Florisil column, NH2 column and C18 column solid phase extraction column for the samples, using capillary column gas chromatography as a detection method, GC-ECD to qualitative analyze. The recovery rate of Cypermethrin is 91.2% ∼ 98% after Cleanert Florisil, the coefficient of variation is 0.53% ~ 3.67%, the detection limit is 0.0015 mg • kg ^-¹. The first day, spraying the fenvalerate, dimethoate, chlorothalonil pesticides residues in lettuce was higher than the greenhouse tomato; pesticides (dimethoate, chlorothalonil, fenvalerate) residues in vegetables were higher than those in the open field, pesticide degradation speed is obviously higher than in greenhouse. Subsidence of pesticide is an important factor affecting greenhouse pesticide residues.

You might also be interested in these eBooks

View Preview

Info:

Periodical:

Applied Mechanics and Materials (Volume 686)

Pages:

73-77

DOI:

https://doi.org/10.4028/www.scientific.net/AMM.686.73

Citation:

Cite this paper

Online since:

October 2014

Authors:

Ru Ling Zhang*

Keywords:

Analysis of Pesticide Residues, Chlorothalonil, Dimethoate, Fenvalerate, Gas Chromatography

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

Citation:

* - Corresponding Author

References

[1] Ma Qinghua, etc. Study of chlorothalonil, cypermethrin and fenvalerate residues in winter jujube [J]. China Agricultural Science Bulletin, 2009, 25 (15): 5154.

Google Scholar

[2] Wang Ping, Wang Qi, Liu Qing, etc. Analysis of 5 pyrethroid pesticide residues in Ganoderma lucidum, poria[J]. Chinese clinical laboratory science, 2007, 13 (1): 57.

Google Scholar

[3] Shi Yajun, Wei Zhaojun, Jia Linfang, etc. Determination of 5 kinds of Pear by high performance liquid chromatography of pyrethroid pesticide multi residues[J]. Journal of Beijing University of Agriculture, 2008, 23 (4): 2528.

Google Scholar

[4] Wei Zhaojun, Shi Y. J, Zhao J. Z, etc. Improvement for analyzing pyrethroids in vegetables by HPLC[J]. Chinese Agricultural Science Bulletin, 2009, 25 (7): 89. 3.

Google Scholar

[5] Wang Xiang, Song Guoxin, Hu Yaoming. Method for extracting pyrethroid pesticide residues in tea GC/MS study[J]. MS Sinica, 2008, 29 (2): 97-100.

Google Scholar

[6] Wu Shengfang, Wang Liping, Liu Yangmang. Accelerated solvent extraction and gas chromatography tandem mass spectrometric determination of 3 pyrethroid pesticide residues in Chrysanthemum[J]. Analysis of the test chamber, 2008, 27 (11): 65-67.

Google Scholar