Microstructural and Tribological Characterization of Atmospheric Plasma-Nitrided HS6-5-2C Tool Steel

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The nitriding process is well known as a method to improve wear, strength and corrosion characteristics of materials surface. The Institute of Materials Science of Leibniz Universität Hannover is on a stage of development of a new nitriding process under atmospheric conditions. The main purpose of the research work is formation of a nitrided layer on the locally loaded areas of a tool (e.g. forging die) under atmospheric conditions to increase wear resistance and durability of operating tools. Nitride layers were generated on the tool steel HS6-5-2C using the transmitted plasma arc. After atmospheric plasma nitriding the samples were investigated using optical microscopy, transmission electron microscopy (TEM), X-Ray diffraction (XRD) and microhardness testing techniques. It has been revealed that the modified zone thickness after atmospheric plasma nitriding reaches 200 μm. TEM and XRD analysis have shown that new phases corresponding to iron nitrides were formed in the surface zone. Microhardness of the surface layer is increased by 10% and friction coefficient has been reduced by approximately 50% in comparison with base material.

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345-350

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December 2014

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© 2015 Trans Tech Publications Ltd. All Rights Reserved

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[1] K. Bobzin, Oberflächentechnik für den Maschinenbau, first ed., Wiley-VCH, Weinheim, (2012).

Google Scholar

[2] F. -W. Bach, T. Duda, Moderne Beschichtungsverfahren, Wiley-VCH, Weinheim, (2000).

Google Scholar

[3] C. Weist, H. Westheide, K. Lange, Application of chemical and physical methods for the reduction of tool wear in bulk metal forming processes, CIRP Annals-Manufacturing Technology. 35 (1986) 199-204.

DOI: 10.1016/s0007-8506(07)61870-8

Google Scholar

[4] T. auf dem Brinke, Plasmagestützte Oberflächenveredelung, Moderne Industrie, Landsberg/Lech, (2006).

Google Scholar

[5] J. Yang, Y. Liu, Z. Ye, D. Yang, S. He, Microstructural and tribological characterization of plasma- and gas-nitrided 2Cr13 steel in vacuum, Mater. Des. 32 (2011) 808-814.

DOI: 10.1016/j.matdes.2010.07.022

Google Scholar

[6] J. Michalski, P. Wach, J. Tacikowski, M. Betiuk, K. Burdynski, S. Kowalski, A. Nakonieczny, Contemporary industrial application of nitriding and its modifications, Mater. Manuf. Processes. 24 (2009) 855–858.

DOI: 10.1080/10426910902844203

Google Scholar

[7] D. Liedtke, Wärmebehandlung von Eisenwerkstoffen, fifth ed., Expert-Verl., Renningen, (2010).

Google Scholar

[8] D. Linse, Oberflächenbehandlung mit Lichtbogenplasmabrennern zur Standmengenerhöhung von Gesenkschmiedewerkzeugen, VDI-Verlag GmbH, Düsseldorf, (1993).

Google Scholar

[9] T. Hassel, C. Birr, F.W. Bach, Surface zone modification by atmospheric plasma-nitriding (APN) with the aid of the transmitted plasma-arc, J. Key Eng. Mat. 438 (2010) 147–154.

DOI: 10.4028/www.scientific.net/kem.438.147

Google Scholar

[10] M. Schaper, Y. Lizunkova, M. Vucetic, T. Cahyono, H. Hetzner, S. Opel, J. Schneider, T. Koch, B. Plugge, Sheet-bulk metal forming a new process for the production of sheet metal parts with functional components, Metallurgical and Mining Industry. 3 (2011).

DOI: 10.1007/s12289-010-0778-0

Google Scholar

[11] Y. Lizunkova, S. Burov, T. Hassel, M.S. Bierbaum, F.W. Bach, Temperature control during the APN-process on the steel 1. 3343, J. Key Eng. Mat. 504-506 (2012) 1017–1022.

DOI: 10.4028/www.scientific.net/kem.504-506.1017

Google Scholar

[12] H. Oettel, H. Schumann, Metallografie, 14 ed., Wiley-VCH, Weinheim, (2005).

Google Scholar

[13] A. Smirnov, Y. Lizunkova, A. Nikulina, T. Hassel, F. -W. Bach, Structure of surface zone of the steel 1. 3343 after atmospheric plasma nitriding, XXIV Russia Conference on electron microscopy (RCEM-2012), Bogorodskiy petschatnik, Moskow, (2012).

Google Scholar

[14] A.A. Chevakinskaya, Ya.S. Lizunkova, A.I. Smirnov, A.A. Nikulina, Formation of high-strength structure in a surface layer of HSS 1. 3343 after saturation by atmospheric plasma nitriding, book abstr., intern. conf. on surface engineering for research and industrial applications, Novosibirsk (2014).

Google Scholar

[15] M. Goldstein, S. Grachev, Yu. Veksler, Special steels, Metallurgy, Moscow, (1985).

Google Scholar