The Synthesis of TiC Powders by Carbothermal Reduction Method in Vacuum

Xue Tan Ren; Yan Chun Liu; Shui Hui Chen; Lai Guang Hou; Guo Long Wang; Yuan Cheng Teng

doi:10.4028/www.scientific.net/AMR.1064.62

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 1064The Synthesis of TiC Powders by Carbothermal...

The Synthesis of TiC Powders by Carbothermal Reduction Method in Vacuum

Abstract:

The TiC powders were synthesized by carbothermal reduction of TiO₂ in vacuum using the titania and carbon black as raw materials. The molar ratio of C to TiO₂ was 3:1. The crystalline phase, microstructure and morphology of the obtained samples were investigated by XRD and SEM. The results show that single-phase and well-crystallized TiC powders were obtained at 1300^°C for 1h when the system pressure was 20 Pa. The particle morphologies are composed of fine grains about 200 nm.

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Periodical:

Advanced Materials Research (Volume 1064)

Pages:

62-65

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.1064.62

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Online since:

December 2014

Authors:

Xue Tan Ren, Yan Chun Liu, Shui Hui Chen, Lai Guang Hou, Guo Long Wang, Yuan Cheng Teng

Keywords:

Carbothermal Reduction Method, Low-Temperature, TiC Powders, Vacuum

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