Synthesis of Nanosized Silica Powder by Ultrasonic Process

Sang Geun Lee; Hyung Sup Kim; Seong Soo Park; Byung Young Moon; Beom Soo Kang; Hee Chan Park

doi:10.4028/www.scientific.net/AMR.11-12.669

Paper Titles

Microstructure and Mechanical Properties of AZ31B Magnesium Alloy Sheets Prepared by Extruding and Rolling
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Influence of Anodizing Process on Cohesive Property of Anodic Films on Aluminum Alloy with Rubber
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Diffusion-Rolling Bonding of Polycrystalline Metal in Two-Phase Region and Effect of Bonding Temperature
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Anodic Oxidation Parameters on Al-Cu Alloy Anodizing Film's Electrochemical Ability by EIS
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Synthesis of Nanosized Silica Powder by Ultrasonic Process
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Synthesis of Hollow Silica Particle by Combination of Bubble Templating Method and Sol-Gel Transformation
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Influence of Inorganic Ion on the Synthesis of Hollow Calcium Carbonate
p.677

Characterization of Heterocoagulation by Direct Observation Technique
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Centrifugal Sintering - Development of a New Pressure Sintering Process -
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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 11-12Synthesis of Nanosized Silica Powder by Ultrasonic...

Synthesis of Nanosized Silica Powder by Ultrasonic Process

Abstract:

Nanosized silica powders were synthesized via w/o emulsion method using sodium silicate as SiO2 source under ultrasonic process. The powders were prepared under conventional process and ultrasonic process using the same reactants at ambient temperature for 1h varying the concentration of Na2SiO3 solution while fixing the concentration of surfactant in cyclohexane. The particle size of the silica powder decreased with decreasing the concentration of sodium silicate solution under both conditions, with and without ultrasounds. However, the particle size and size distribution of the silica powder with ultrasounds were smaller and narrower than those without ultrasounds, establishing that ultrasound treatments decrease the particle size and become narrow in particle size distribution.

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Periodical:

Advanced Materials Research (Volumes 11-12)

Pages:

669-672

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.11-12.669

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Online since:

February 2006

Authors:

Sang Geun Lee, Hyung Sup Kim, Seong Soo Park, Byung Young Moon, Beom Soo Kang, Hee Chan Park

Keywords:

Nano-Size, Powder, Silica, Synthesis, Ultrasonic Process

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References

[1] H. Gleiter: Acta Mater. Vol. 48 (2000), p.1.

Google Scholar

[2] Y. Zhu. C. Ding, G. Ma and Z. Du: J. Solid State Chem. Vol. 139 (1988), p.124.

Google Scholar

[3] S.T. Bromley and E. Flikkema: Chem. Phys. Lett. Vol. 278 (2003), p.622.

Google Scholar

[4] C.V. Suciu, T. Iwatsubo and S. deki: J. Colloid Interface Sci. Vol. 259 (2003), p.62.

Google Scholar

[5] M. Lee, C.Y. Tai and C. Lu: J. Eur. Ceram. Soc. Vol. 19 (1999), P. 2593.

Google Scholar

[6] M. Chatterjee and A. Patra: J. Am. Ceram. Soc. Vol. 84 (2001), p.1439.

Google Scholar

[7] I. Capek: Adv. Colloid Interface Sci. Vol. 10 (2004), p.49. 0. 0 0. 5 1. 0 1. 5 2. 0 2. 5 3. 0 3. 5.

Google Scholar

[10] [20] [30] [40] [50] [60] Frequency(%) Particle size(µµµµm) d=1. 05µµµµm (a) 0. 0 0. 5 1. 0 1. 5 2. 0 2. 5 3. 0 3. 5.

Google Scholar

[10] [20] [30] [40] [50] [60] (b) Frequency(%) Particle size (µµµµm) d=0. 17µµµµm Fig. 5. Particle size distributions of SiO2 powders synthesized with 0. 5M Na2SiO3 under (a) conventional process and (b) ultrasonic process.

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