Solution Spray Controlled Polymorph Selective Synthesis of Lead Chrome Nanocrystals

Ujwal D. Patil; Virendra J. Patil; Ravindra D. Kulkarni

doi:10.4028/www.scientific.net/AMR.1110.263

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 1110Solution Spray Controlled Polymorph Selective...

Solution Spray Controlled Polymorph Selective Synthesis of Lead Chrome Nanocrystals

Abstract:

The controlled solution spray process with superior molecular contacting between finely atomized reactants in impinging solution spray reactor was carried out with an objective to develop the nonionic surfactant (Tween-80) mediated coprecipitation protocol for the polymorph selective synthesis of lead chrome (PbCrO₄) nanocrystals. Monoclinic PbCrO₄ nanorods with size in the range of 37.8-51.9 nm at Tween-80 loadings of 2-10 g/L were obtained. The functional group, surfactant adsorption, crystal type, size and morphology of the PbCrO₄ nanocrystals were determined by FTIR, XRD and FESEM analysis.

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Periodical:

Advanced Materials Research (Volume 1110)

Pages:

263-266

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.1110.263

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Online since:

June 2015

Authors:

Ujwal D. Patil*, Virendra J. Patil, Ravindra D. Kulkarni

Keywords:

Atomization, Lead Chrome Nanocrystals, Polymorph, Solution Spray Reactor

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