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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 146-147Direct Deoxidation of ZrOCl2 Powder to Zirconium...

Direct Deoxidation of ZrOCl₂ Powder to Zirconium With Non-Sintering

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Abstract:

Direct electro-deoxidation of zirconium oxychloride powder without sintering in molten CaCl2 and NaCl mixture salt was studied. Molten CaCl2 and NaCl mixture salt as electrolyte, a little graphite crucible filled with zirconium oxychloride powder as novel cathode and a graphite rod as anode, deoxidation experiments were performed at 700 and 3.2V for 8h and 15h, respectively. Results show that using new material of zirconium oxychloride and the method of direct electro-deoxidation without sintering can be applied to the preparation of fine zirconium metal particles, which have a great advantage in cheap cost, short technical process, and energy saving.

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Advances in Superalloys

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Periodical:

Advanced Materials Research (Volumes 146-147)

Pages:

775-779

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.146-147.775

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Online since:

October 2010

Authors:

Xiang Yu Zou, Hong Wei Xie, Yu Chun Zhai, Xiao Chuan Lang

Keywords:

CaCl₂-NaCl, Direct Electro-Deoxidation, Non-Sintering, Zirconium, Zirconium Oxychloride

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© 2011 Trans Tech Publications Ltd. All Rights Reserved

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