Preparation of Silica Nanoparticles Using Silica-Rich Filtrate from Potassium-Rich Rock

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Abstract:

The silicon-rich filtrate which was obtained from the desilication solution of potassium-rich rock was used as raw materials to prepare nanometer sillica and ultrasonic dispersion method was applied to the chemical precipitation process. A detailed study was carried out on the effect of filtrate concentration, surfactant dosage, reaction temperature, calcinations temperature, ultrasonic dispersion on size of silica nanoparticles. The basic properties and size of particles were characterized by means of FE-SEM, TEM, XRD, TGA and FTIR. The results obtained in the study indicated that monodisperse and uniform-size silica nanoparticles were prepared using ultrasonication by chemical precipitation process and the average particle size was 50 nm.

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Advanced Materials Research (Volumes 160-162)

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1372-1377

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November 2010

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© 2011 Trans Tech Publications Ltd. All Rights Reserved

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[1] T. Jesionowski: Powder Tech. Vol. 127 (2002), pp.56-65.

Google Scholar

[2] J. Wacker, V.K. Parashar and M.A.M. Gijs: Procedia Chemistry. Vol. 1 (2009), pp.377-380.

Google Scholar

[3] W. Stöber, A. Fink and E. Bohn: J. Colloid Interface Sci. Vol. 26 (1968), pp.62-69.

Google Scholar

[4] R. Lindberg, J. Sjoblom and G. Sundholm: Colloids Surf. Vol. A99 (1995), pp.79-84.

Google Scholar

[5] K.S. Rao, K. El-Hami, T. Kodaki, K. Matsushige and K. Makino: J. Colloid Interface Sci. Vol. 289 (2005), pp.125-130.

DOI: 10.1016/j.jcis.2005.02.019

Google Scholar

[6] A. van Blaaderen, J. van Geest and A. Vrij: J. Colloid Interf. Sci. Vol. 154 (1992), pp.481-485.

Google Scholar

[7] R. Lindberg, J. Sjöblom and G. Sundholm: Colloids Surf. Vol. A99 (1995), pp.79-84.

Google Scholar

[8] H. Giesche and J. Europ: Ceram. Soc. Vol. 14 (1994), pp.189-192.

Google Scholar

[9] J.D. Wells, L.K. Koopal and A. de Keizer: Colloids Surf. Vol. A166 (2000), pp.171-173.

Google Scholar

[10] D.G. Shchukin and G.B. Sukhorukov: Adv. Mater. Vol. 16 (2004), pp.671-674.

Google Scholar

[11] C. Barbé, J. Bartlett, L. Kong, K. Finnie, H.Q. Lin, M. Larkin, S. Calleja, A. Bush and G. Calleja: Adv. Mater. Vol. 16 (2004), p.1959-(1965).

DOI: 10.1002/adma.200400771

Google Scholar

[12] V.T. John, B. Simmons, G.L. McPherson, A. Bose and Curr. Opin: Colloid Interface Sci: Vol. 7 (2002), pp.288-293.

Google Scholar

[13] G.H. Gogush and C.F. Zukoski: J. Colloid Interface Sci. Vol. 142 (1991), pp.1-6.

Google Scholar